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Internal flow behaviour and microstructural evolution of the bobbin-FSW welds: thermomechanical comparison between 1xxx and 3xxx aluminium grades

Tamadon Abbas, Pons Dirk J., Sued Kamil, Clucas Don

Advances in Materials Science

2021

Vol. 21, nr 2(68)

40--64

The influences of processing parameters and tool feature on the microstructure of AA1100 and AA3003 aluminium alloys were investigated using bobbin friction stir welding (BFSW). The research includes flow visualization and microstructural evolution of the weld texture using the metallographic measurement method. Results indicated that the operational parameters of the welding (e.g. feed rate, rotating speed) and the geometry of the tool can directly affect the flow patterns of the weld structure. The microscopic details revealed by the optical and electron microscope imply the dynamic recrystallization including grain refinement and precipitation mechanisms within the stirring zone of the weld region. The microscopic observations for the weld samples show a better performance of the fully-featured tool (tri-flat threaded pin and scrolled shoulders) compared to the simple tool without inscribed surface features. The fully-featured tool resulted in a more uniform thermomechanical plastic deformation within the weld structure along with the precipitation hardening and the homogeneity of the microstructure.

Effects of TiO2/SiO2 reinforced nanoparticles on the mechanical properties of green hybrid coating

Gobara M.

International Letters of Chemistry, Physics and Astronomy

2015

Vol. 47

56--66

Titanium and silica oxides nanoparticles were introduced into hybrid silica sol–gel/epoxy coating to enhance the mechanical properties of coatings. Titanium dioxide (TiO2) and silica oxide (SiO2) were chemically synthesised before adding to the prepared silica sol gel coating. X-ray diffraction (XRD), Energy-dispersive x-ray analysis (EDX) and Transmission Electron microscope (TEM) were used to characterize the prepared nanoparticles. The coating was then applied to 3003 aluminium alloy (AA3003) surface. The adhesion performance of different sol gel coating compositions was investigated using shear test to define the influence of nanoparticles on adhesive strength of the coating. The Rockwell C hardness test was used to study the micro-hardness of different compositions of sol gel coating. Also, contact angel was used to investigate the hydrophobicity of the coatings. The results showed that there was a significant improvement of the adhesion performance of hybrid silica sol gel coating due to addition of TiO2 and the hydrophobicity of sol gel coating was increased due to addition of SiO2 nanoparticles.