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Reverse flotation of iron ore using amphoteric surfactant: 2-((2(decyloxy)ethyl)amino)lauric acid

Luo Binbin, Zhu Yimin, Sun Chuanyao, Li Yanjun, Han Yuexin

Physicochemical Problems of Mineral Processing

2021

Vol. 57, iss. 3

73--83

2-((2-(decyloxy)ethyl)amino)lauric acid (C10H21CH(NH(CH2)3OC10H21)COOH, (LDEA), a novel amphoteric surfactant, has been first utilized as the collector for on-site the reverse flotation of Anqian mixed magnetic concentrates. The separation performances were investigated systematically by flotation conditioning tests, open-circuit flowsheet experiment, and locked cycle flowsheet test. The flotation condition test's results showed that the optimal roughing conditions were pulp pH of 10, starch dosage 1000 g/Mg, and LDEA dosage of 500 g/Mg at 25 °C. Under the optimized flotation conditions, through one roughing - three scavengings locked cycle flowsheet, the iron concentrate with a total iron grade of 68.08% and recovery of 88.20% was obtained. In contrast, the iron grade of the tailings was only 12.32%. Compared with the flotation results of anionic commercial surfactant RA-715 used as the collector, the LDEA has a better separation performance. The iron grade and recovery increased by 0.07% and 0.86% in the iron concentrate, and the grade of the tailings decreased 3.72%, respectively. Besides, the LDEA possesses more advantages, such as a simple flotation process, no activator (CaO) addition, lower collector consumption, and lower pulp temperature. The study revealed that the novel amphoteric surfactant LDEA was an effective flotation collector with good collecting and separation ability on natural iron ores at a comparatively lower temperature.

Molecular dynamic simulations study of 2-((2- (decyloxy)ethyl)amino)lauric acid adsorption on the α-quartz (1 0 1) surface

Luo Binbin, Zhu Yimin, Sun Chuanyao, Li Yanjun, Han Yuexin

Physicochemical Problems of Mineral Processing

2019

Vol. 55, iss. 5

1209--1216

Adsorption mechanism of a novel amphoteric collector 2-((2-(decyloxy)ethyl)amino)lauric acid (CH3(CH2)9CH(NH(CH2)3-O-(CH2)9CH3)COOH, LDEA) on the α-quartz (1 0 1) surface has been investigated through molecular dynamic (MD) simulation calculations at a molecular level. The adsorption process showed that the LDEA collector could be adsorbed onto α-quartz’s (1 0 1) surface as the H atom in the polar carboxyl and amino functional group of the collector moved closer to the O atom of quartz (1 0 1) surface. The interaction energies of the collector LDEA molecule and its ionic derivative species on α-quartz surfaces in vacuum and aqueous solutions are in the order of pH 4 < pH 12 < in vacuum < pH 10 < pH 6, which demonstrating that the α-quartz (1 0 1) surface could absorb the collector LDEA in the forms of electrostatic and hydrogen bonding interactions. It also reveals that the optimal pulp pH range for LDEA adsorption on α-quartz’s surface is between neutral and weak alkali environment (pH 6 - 10). The trend obtained from molecular modeling has been validated by microflotation studies on quartz at different pHs.