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Preparation and characterisation of (meth)acryloyloxystarch

Stawski D., Jantas R.

Autex Research Journal

2003

Vol. 3, no. 2

85--89

By Schotten-Bauman's esterification of starch with (meth)acryloyl chlorides, an ester derivative of starch - (meth)acryloyloxystarch - was prepared, which contains double bonds. The original starch and (meth)acryloyloxystarch were characterised by FTIR, 1H-NMR, 13C-NMR, GPC and TGA. (Meth)acryloyloxystarch was polymerised in solution by the free-radical process and by photopolymerisation in a solid state to obtain a crosslinked product.