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Consolidation and Oxidation of Ultra Fine WC-Co-HfB2 Hard Materials by Spark Plasma Sintering

Park Hyun-Kuk, Oh Ik-Hyun, Kim Ju-Hun, Hong Sung-Kil, Lee Jeong-Han

Archives of Metallurgy and Materials

2021

Vol. 66, iss. 4

997--1000

In this study, a novel composite was fabricated by adding the Hafnium diboride (HfB2) to conventional WC-Co cemented carbides to enhance the high-temperature properties while retaining the intrinsic high hardness. Using spark plasma sintering, high density (up to 99.4%) WC-6Co-(1, 2.5, 4, and 5.5 wt. %) HfB2 composites were consolidated at 1300°C (100°C/min) under 60 MPa pressure. The microstructural evolution, oxidation layer, and phase constitution of WC-Co-HfB2 were investigated in the distribution of WC grain and solid solution phases by X-ray diffraction and FE-SEM. The WC-Co-HfB2 composite exhibited improved mechanical properties (approximately 2,180.7 kg/mm2) than those of conventional WC-Co cemented carbides. The high strength of the fabricated composites was caused by the fine-grade HfB2 precipitate and the solid solution, which enabled the tailoring of mechanical properties.

Effect of Deflector Plate for Particle Size Segregation Control

Kim Kang-Min, Kim Ju-Hun, Kwon Jae-Hong, Lee Ji-A, Han Jeong-Whan

Archives of Metallurgy and Materials

2019

Vol. 64, iss. 2

495--500

In general, uniform mixing of particles is desirable in the process of particle handling. However, during the charging of sinter feed and upper ore, size segregation must be induced to prevent heat imbalance, ensure bed permeability, and prevent the loss of fine ore. In this study, upper ore charging was simulated using a discrete element method (DEM) to find the optimal method for controlling particle size segregation, and the segregation characteristics in the upper ore bed were investigated when a deflector plate was applied to the charging machine. The degree of vertical segregation increased when a deflector plate was applied, and it was confirmed that the segregation direction in the upper ore bed can be controlled by adjusting the charging direction of the upper ore by using a deflector plate. In order to apply this method directly to the actual process, further study is needed to understand the influence of the characteristics of the deflector plate such as length and angle.