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Beneficial effects and mechanism of lead ion on wolframite flotation

Yang S., Qiu X., Peng T., Chang Z., Feng Q., Zhong C.

Physicochemical Problems of Mineral Processing

2016

Vol. 52, iss. 2

855--873

In this study the effects and mechanism of lead ions influence on wolframite flotation with benzohydroxamic acid (BHA) were studied through micro-flotation, adsorption experiments, zeta potential measurements, logarithmic concentration diagram, and X-ray photoelectron spectroscopy. It was observed that lead ions could significantly enhance the recovery of wolframite in flotation and adsorption density of collector BHA onto the wolframite surface. The results showed that Pb existed in the forms of lead ion, monohydric lead, and lead hydroxide at the water-wolframite interface respectively, at three pH ranges. They increased the zeta potential of wolframite. However, the zeta potential of wolframite was still negative, resulting in repulsive electrostatic force to anionic collector BHA. Combining with XPS spectra, it revealed the chemisorption of BHA onto the wolframite surface. In addition, PbO or Pb(OH)2 was observed on the wolframite surface due to the reaction between lead ions and wolframite. These reaction products increased the adsorption site of BHA on the wolframite surface because Pb-hydroxamate was found on the wolframite surface.

Recovery mechanisms of sericite in microcrystalline graphite flotation

Li H., Ou L., Feng Q., Chang Z.

Physicochemical Problems of Mineral Processing

2015

Vol. 51, iss. 2

387--400

Sericite is the main contaminant of concentrate in commercial microcrystalline graphite ore flotation. It was necessary to identify its recovery mechanisms so that the appropriate solution can be selected. In this study, the influence of sericite on flotation selectivity of microcrystalline graphite ore and its recovery mechanisms were investigated. Artificial mixtures flotation test suggested that sericite seriously reported into concentrate leading to poor flotation selectivity of microcrystalline graphite ore. However, the aggregation/dispersion behavior of artificial mixtures indicated that a large repulsive energy existed between sericite and microcrystalline graphite particles at pH 7.4, and sericite was not likely to report into graphite concentrate by slime coating. The results obtained from contact angle measurements and a technique of Warren showed that the floated sericite reached the froth via a combination of both entrainment and entrapment mechanisms, not via true flotation.