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Direct Room-Temperature Synthesis of Ni(Hdmg)2 Nanorods

Li C. H., Cao Y. X., Wang J. T., Zhang A. F.

Polish Journal of Chemistry

2009

Vol. 83, nr 2

175-180

A simple and fast route based on microemulsion synthesis approach was developed to synthesis one-dimensional (1D) nanostructures of Ni(Hdmg)2 (H2dmg = dimethyl-glyoxime) using nickel chloride and H2dmg as reactants. Scanning electron microscopy (SEM), transmission electron microscope (TEM), IR spectra and elemental analysis were adopted to characterize the as-prepared Ni(Hdmg)2 nanostructures. The sizes of as-prepared nanorods can be adjusted easily and the formation mechanism was proposed tentatively. The successful synthesis of Ni(Hdmg)2 nanorods provide a convenient avenue for tailoring nanocrystals of complexes containing organic groups that are sensitive to temperature.