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FMR study of samples obtained by nitriding and nitrides reduction of nanocrystalline iron

Typek J., Guskos N., Zolnierkiewicz G., Guskos A., Kielbasa K., Pelka R., Arabczyk W.

Materials Science Poland

2016

Vol. 34, No. 1

6--12

Samples obtained by nitriding of promoted nanocrystalline iron and the nitrides reduction at various nitriding potential in terms of thermodynamic parameters were investigated by electron paramagnetic resonance/ferromagnetic resonance (EPR/FMR) method at room temperature. Experimental FMR spectra were fitted by the Dysonian-type resonance lines arising from the presence of different Fe–N phases. The obtained FMR parameters allowed us to identify the component phases and to determine their magnetic properties. In general, the proposed simple method of decomposition of the FMR spectra produced results on the phase content in investigated samples that were consistent with XRD measurements and additionally, magnetic characteristics of the studied nanomagnets.

Magnetic characterization of nanocrystalline iron samples with different size distributions

Typek J., Zolnierkiewicz G., Pelka R., Kielbasa K, Arabczyk W, Guskos N.

Materials Science Poland

2014

Vol. 32, No. 3

423—429

Nanocrystalline iron was obtained by fusing magnetite and promoters. The oxidized form was reduced with hydrogen and passivated (sample P0). The average nanocrystallite size in sample P0 was d(P0) =16 nm and the width of size distribution was s(P0) = 18 nm. Samples of nanocrystalline iron with narrower diameter ranges and larger and smaller average crystallite sizes were also synthesized. They were: sample P1 (d(P1) = 28 nm, s(P1) = 5 nm), sample P2 (d(P2) = 22 nm, s(P1) = 5 nm), sample P3 (d(P3) = 12 nm, s(P1) = 9 nm). These four samples were studied at room temperature by dc magnetization measurements and ferromagnetic resonance at microwave frequency. Correlations between samples sizes distributions (average size and width of the sizes) and magnetic parameters (effective magnetization, anisotropy field, anisotropy constant, FMR linewidth) were investigated. It was found that the anisotropy field and effective magnetization determined from FMR spectra scale linearly with nanoparticle sizes, while the effective magnetic anisotropy constant determined from the hysteresis loops decreases with nanoparticle size increase.