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Influence of synthesis conditions on the properties of FeXCoYOZ - nanoparticles in SiO2Sol-gel film

Sidsky V. V., Gaishun V. E., Demidenko O. M., Savitskaya T. A., Panykov V. V., Semchenko A. V.

Journal of Automation Mobile Robotics and Intelligent Systems

2009

Vol. 3, No. 4

91-92

Synthesis conditions influence on structure of FexCoyOz - nanoparticle in SiO2 - sol-gel coating is discussed. The samples are synthesized by hybrid sol - gel method including following stages: TEOS hydrolysis, introduction into sol of Co(NO3)2 . 6H20 and Fe(NO3)3 . 9H20, deposition of film-forming sol by spin-coating on silica substrate, heat treatment at the temperature from 200 up to 900 °C. The Synthesis conditions influence on a specific structural property of sol gel films is investigated by AFM.