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Chemical properties of hydroxyapatite deposited through electrophoretic process on different sandblasted samples

Gradinariu I, Stirbu I, Gheorghe C A, Cimpoesu N, Agop M, Cimpoesu R, Popa C

Materials Science Poland

2014

Vol. 32, No. 4

578--582

An implantable material based on titanium (Ti6Al4V) was sandblasted in order to be deposited with a thin film of hydroxyapatite. Two samples of the alloy, in a shape of a bar with 10 mm diameter and 20 mm length, were subjected to mechanical treatment. After deposition of the hydroxyapatite through electrophoresis process, the samples were analyzed by scanning electron microscopy. The nature and chemical properties of thin films formed on Ti-based substrate were investigated with electrochemical impedance spectroscopy based on the extremely high polarization resistance of the material. The results revealed the formation of a homogeneous layer on the surface of the metallic substrate. The layer composed of TiO2 and hydroxyapatite provided a high corrosion protection.

Oxidation of an austenitic stainless steel pipe contaminated by petroleum products

Palamarciuc I., Galușcă D. G., Agop M, Achiței D., Manoliu Nuțescu Duduman C.

Journal of Achievements in Materials and Manufacturing Engineering

2014

Vol. 62, nr 2

63--68

Purpose:The experimental researches of this paper were carried out in order to investigate the characteristics of the oxide layers obtained on the internal and external surfaces of an austenitic stainless steel pipe. Design/methodology/approach: The surfaces of an austenitic stainless steel pipe were investigated by Scanning Electron Microscopy (SEM), Energy-dispersive X-ray spectroscopy (EDX) and X-ray diffraction (XRD) analysis. Also the microindentation hardness was measured, on the both surfaces and between them, in order to detect and verify the improvement of the mechanical properties. Findings: The external surface did not present any corrosion results but the internal surface of the analysed pipe was contaminated by sulphur during the transportation of petroleum products. In spite of this fact it was found that the mechanical properties of such a surface can be improved by air oxidation Researches limitations/implications: It was found that oxidation at lower temperatures (300°C) resulted in formation of harder coatings. For comparison and better interpretation this paper presents the results of the analysis and measurements performed before and after the oxidation and cleaning, demonstrating the effectiveness of this simple method of reconditioning. Originality/value: By experimental investigations of the physical, chemical and mechanical properties of the oxide layers, obtained on J92603 austenitic stainless steel by thermal oxidation, we demonstrated the principled technological possibility of obtaining hardening thermal oxide layers on corroded pipes’ surface.