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Zinc oxide nanoparticles as photo-catalytic and anti-bacterial pigment for alkyd resin based coating

Kavitha Sri A., Sivaraj M., Rajkumar S., Ruby Shelin A., Sajitha L.P., Jeyasubramanian K., Jeen Robert R.B., Hikku G.S.

Archives of Materials Science and Engineering

2022

Vol. 118, nr 1

29--35

Purpose: Recently, there has been an upsurge among people around the world in maintaining a sustainable and hygienic environment. This is due to the over-exploitation of recourses causing environmental pollution and spreading bacterial infections. In this regard, scientists are motivated to develop smart coatings where environmental pollutants and bacterial cells are degraded when in contact with their surfaces. Design/methodology/approach: In our previous report, ZnO nanoparticles (NPs) were prepared using the precipitation technique, showing good photocatalytic and antibacterial activity [1]. In this context, the present study details the use of ZnO NPs as pigment for the fabrication of alkyd resin-based self-cleaning coating. The coating was developed by mixing ZnO NPs and alkyd resin along with the additives using the ball milling technique. The developed coating was characterized using field emission scanning electron microscopy, energy dispersive X-ray spectroscopy, atomic force microscopy, and water contact angle measurements. Findings: To elucidate the self-cleaning and hygienic behaviour of the ZnO/alkyd resin coating, the dried coating was exposed to crystal violet (CV) solution as a model dye pollutant and bacterial strains to assess its photocatalytic and antibacterial activity. The droplets of CV solution placed over the coating almost degraded after 360 min of exposure to sunlight owing to the presence of ZnO NPs in the coating. Further, the coating exhibits reasonable antibacterial activity against E. coli and P. aeruginosa whereas it displays low antibacterial activity against S. aureus. Research limitations/implications: Even though, the self-cleaning coating shows promising results, tuning the activity of the photo-catalytic pigment can improve the pollutant degradation efficiency and elevate bactericidal activity. Originality/value: ZnO NPs-impregnated alkyd resin coating for self-cleaning applications is novel.

Optimization on friction and wear behaviour of Al-Si alloy reinforced with B4C particles by Powder Metallurgy using Taguchi design

Jeya Raj R., Lenin Anselm W. A., Jinnah Sheik Mohamed M., Christopher Ezhil Singh S., John T. D., Rajeev D., Glan Devadhas G., Jaya Christyan K. G., Malkiya Rasalin Prince R., Jeen Robert R. B.

Bulletin of the Polish Academy of Sciences. Technical Sciences

2020

Vol. 68, nr 6

1393--1402

This research paper discusses the friction and wear behaviour of Al-12Si alloy reinforced with B4C prepared through Powder Metallurgy (P/M) method by varying the weight percentage of reinforcement (x = 2, 4, 6, 8, and 10) content. The samples were prepared by using die and punch assembly and the lubricant used to eject the sample from the die was molybdenum disulfide. The compaction was done by using a compression testing machine by applying a pressure of 800 MPa. The dry sliding friction and wear behaviour of the sample was conducted on a Pin-on-Disc machine and the experimental values of friction and wear were calibrated. The Taguchi design experiment was done by applying an L25 orthogonal array for 3 factors at 5 levels for the response parameter Coefficient of Friction (CoF) and wear loss. The SEM images show the shape, size and EDX confirm the existence of Al, Si, B4C particles in the composites. Analysis of Variance (ANOVA) for CoF of S/N ratio, shows that the reinforcement having 34.92% influence towards the S/N ratio of CoF, ANOVA for wear loss of S/N ratio shows that the sliding distance having 46.76% influence towards the S/N ratio of wear loss, when compared to that of the other two input parameters. The interaction line plot and the 2Dsurface plot for CoF and wear loss show that the increase in B4C content decreases the wear loss and CoF. The worn surface shows that the B4C addition will increase the wear resistance.