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Effect of periphery fixity on ballistic limit of thin aluminum plate subjected to blunt and ogival projectile impact

Tiwari G., Iqbal M. A., Gupta P. K.

International Journal of Applied Mechanics and Engineering

2014

Vol. 19, no. 2

379--395

Three-dimensional numerical simulations were carried out with the ABAQUS/explicit finite element code to study the influence of target boundary conditions on its ballistic limit. 1mm thick 1100-H12 aluminum target of 255 mm span diameter was hit by 19 mm diameter and 50.8 mm length blunt nosed projectile. The mass of the projectile was kept as 52.5 gm. The boundary condition effects on the ballistic limit were investigated by varying the target periphery boundary condition as fully clamped and partially clamped target (75%, 50% and 25%) subjected to projectile impact. The energy absorption and ballistic limit of the target was found to be significantly affected by the boundary conditions. Some of the finite element analysis results were compared with experimental and numerical results reported in international literature and a good agreement between the two was found.

Development and validation of a TLC-densitometric method for the simultaneous quantitation of icariin and L-arginine from commercial formulations

Gupta P. K, Kuber V. V, Ghosh V. K, Bhope S. G, Sharma V., Purohit S

Acta Chromatographica

2011

Vol. 23, no. 3

447--458

A simple, rapid, and specific thin layer chromatographic (TLC) method has been developed and validated for the simultaneous estimation of icariin and L-arginine from commercial polyherbal formulations for sexual dysfunction. The separation of the methanol extract of these formulations was achieved on silica gel 60 F254 aluminum backed TLC plates by using ethyl acetate-acetone-glacial acetic acid-formic acid-water 12:2:1:2:2 (υ/υ) as mobile phase. Densitometric analysis of icariin and L-arginine was monitored in absorbance mode at 270 and 195 nm, respectively. The linear regression analysis data for the calibration plots for icariin and L-arginine showed good linear relationship with r2 = 0.9984 +- 0.01 and 0.9968 +- 0.02, in the concentration ranges of 250–750 and 500–1500 ng/spot, respectively. The method was validated for precision, robustness, and recovery. The average percentage recovery was found to be 98.26% for icariin and 99.63% for L-arginine. The limits of detection and quantitation were 72, 116 and 238, 383 ng/spot, respectively, for icariin and L-arginine. Statistical analysis proves that the method is repeatable and selective for the estimation of the targeted drugs. Since the proposed mobile phase effectively resolves the icariin and L-arginine, this method can be applied for the identification and quantitation of these components in herbal extracts and marketed formulations.