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An innovative technology for recovery of zinc, lead and silver from zinc leaching residue

Zheng Y.-X., Lv J.-F., Liu W., Qin W.-Q., Wen S.-M.

Physicochemical Problems of Mineral Processing

2016

Vol. 52, iss. 2

943--954

Zinc leaching residue is a good source of zinc and has a great potential to be utilized. However, it is very difficult to recover lead, zinc and silver from the residue by traditional technologies. In this study, a new technology based on conversions of PbSO4 and ZnSO4 in the residue to their respective sulfides by reduction roasting with coal powder followed by a flotation treatment was developed. The effects of roasting temperature, coal dosage, reaction time and pyrite dosage were investigated at a laboratory scale. The results showed that the conversion extent of PbSO4 and ZnSO4 under the optimal experimental conditions was 71.89 and 69.76%, respectively. A flotation concentrate containing 39.13% Zn, 6.93% Pb and 973.54 g/Mg Ag was obtained from the treated material, and the recovery of Zn, Pb and Ag was 48.38, 68.23 and 77.41%, respectively. The tailing containing ZnFe2O4 or Fe3O4 could be either stockpiled or further disposed.

Selective reduction of PbSO4 to PbS with carbon and flotation treatment of synthetic galena

Zheng Y.-X., Liu W., Qin W.-Q., Han J.-W., Yang K., Luo H.-L.

Physicochemical Problems of Mineral Processing

2015

Vol. 51, iss. 2

535--546

In order to recover lead from the zinc leaching residues, a new technology involving selective reduction of lead sulfate to lead sulfide with carbon followed by flotation was investigated. The reduction thermodynamics of PbSO4 was discussed and the effects of molar ratio of C to PbSO4, reaction temperature and time were examined by thermogravimetry (TG) and XRD. Verification tests were further carried out to prove the conclusions of thermodynamic and TG analyses, and the transformation extent could reach 86.45% under the optimal roasting conditions. The prepared galena was then subjected to micro-flotation tests, and the highest lead recovery could reach up to 75.32%.