Differential thermal analysis, X-ray diffraction, and metallography were used to study the interaction between the components of the quasi-ternary CdSe–Ga2Se3–Sb2Se3 system. Phase diagrams of three vertical sections, an isothermal section at 670K, aswell as a projection of the liquidus surface have been constructed. The type of mono- and invariant processes in the system has been investigated and the coordinates of invariant points have been determined. Present results can be employed for the growth of CdGa2Se4 single crystals from non-stoichiometric melts.
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