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2 Bulletin of the Polish Academy of Sciences. Chemistry

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Large-amplitude molecular motions in solid metallorganic compounds. Selected X-ray diffraction and 13C CP-MAS NMR spectroscopic investigations

Domalewski W., Riddell F. G.

Bulletin of the Polish Academy of Sciences. Chemistry

1999

Vol. 47, No. 1

41-66

Representative examples of large-amplitude dynamic phenomena in various classes of solid metallorganic compounds are presented. The application of X-ray diffraction measurements and variable-temperature high-resolution NMR spectroscopy for in-vestigation of these motions is described. Advantages and disadvantages of these methods and their complimentary character are shown.

NMR spectroscopic investigations on molecular dynamics in the solid state

Domalewski W., Riddell F. G., Stefaniak L.

Bulletin of the Polish Academy of Sciences. Chemistry

1998

Vol. 46, No. 1

35-59

Representative examples of various large amplitude solid state dynamic phenomena are given. Several NMR techniques suitable for quantitative investigations of such processes are presented. The compability between X-ray diffraction and solid state NMR spectroscopy is pointed out. Common labile character of organic solids is discussed.