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2 Physicochemical Problems of Mineral Processing

2 2020

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Study on gas holdup characteristics of micro-bubble countercurrent contacting flotation column

Han Jikang, Wang Weizhi, Li Ran

Physicochemical Problems of Mineral Processing

2020

Vol. 56, iss. 4

665--675

In order to explore the gas holdup distribution of the microbubble countercurrent contact flotation column in the hematite column cationic reverse flotation process, respectively using conductance method and pressure drop method for air and water as experimental medium characteristics research of flotation column, the research group carries on the gas holdup, examines the aeration quantity, the fill medium and cation collector alkyl polyamine ether (An amine collector―GE609 which consists of four elements: carbon, hydrogen, oxygen and nitrogen)within the column on the influence of the axial and radial gas holdup. The results show that the axial gas holdup from the bottom of the column to the top of the column increases with the increase of height in the range of 0.050.07dm3/s. The radial distribution of gas holdup generally shows the distribution law of “intermediate high, low on both sides”. After the filling medium is added into the column, the radial gas holdup is evenly distributed compared with the empty column, and the gas holdup is increased. Due to the high foaming performance of GE-609, the gas holdup in the column can be increased by changing the amount of aeration and the concentration of the reagent, which can exceed 60% at the maximum. Like other alcohol foaming agents, as time passes, the effect of GE-609 weakens and the gas holdup in the column gradually decreases. The addition of quantitative HCl can improve the foaming performance of GE-609, and the gas holdup in the column is significantly improved and the stability is enhanced.

Study on bubble characteristics of flotation column in hematite reverse cationic flotation process

Wang Weizhi, Han Jikang

Physicochemical Problems of Mineral Processing

2020

Vol. 56, iss. 1

64--75

In the self-designed flotation column simulation system, the foaming characteristics of the micro-bubble countercurrent contact flotation column used in the hematite cation column flotation process are systematically studied. The objective of this study is to investigate the bubble generation by a bubble generator in the flotation column. The bubble image was obtained by the high-speed camera recorder, and the bubble diameter was calculated and analyzed by image processing software. The distribution characteristics of the bubble size under different aeration conditions and with different reagent concentrations were investigated. The results show that as the aeration increases, the average diameter bubbles increases, the bubble size distribution changes from narrow to wide, and the number of small bubbles decreases. The cationic collector GE-609 can change the bubble shape. As the concentration increases, the bubble shape gradually changes from an irregular shape to a standard spherical shape. When the concentration of GE-609 exceeds 2.5 mg/dm3, the average circularity C of the bubbles in the bubble group stabilizes at 1, and the increase in concentration no longer changes the bubble shape. GE-609 also has an efficient foaming effect, as the concentration increases, the bubble diameter distribution changes significantly, the proportion of small bubbles increases, and the proportion of large bubbles decreases significantly. When the critical concentration is exceeded, the bubble diameter distribution probability density peak width no longer changes significantly. Compared with the two types of alcohol foaming agents, GE-609 produces a bubble Sauter diameter close to that of 2-octanol and slightly lower than terpineol.