Synthesis and Characterization of Ionic Cu(I) Perfluorocarboxylate Compounds with 1,4-Bis(diphenylphosphino)butane

Szymańska, I.; Pazderski, L.; Kucharek, R.; Szłyk, E.

Artykuł - szczegóły

Tytuł artykułu

Synthesis and Characterization of Ionic Cu(I) Perfluorocarboxylate Compounds with 1,4-Bis(diphenylphosphino)butane

Autorzy

Szymańska I. , Pazderski L. , Kucharek R. , Szłyk E.

Identyfikatory

Warianty tytułu

Języki publikacji

Abstrakty

A series of ionic Cu(I) perfluorocarboxylate compounds with 1,4-bis(diphenyl - phosphino)bu tane (dppb) of gen eral formula [Cu(dppb)2](RCOO), where R = C2F5, C3F7, C4F9, C6F13, C8F17, was prepared and characterized with MS, IR and 1H, 13C, 19F, 31P NMR spectroscopy. The studied species contained monomeric, bis-chelated [Cu(dppb)2]+ cations and uncoordi nated RCOO- anions. The Cu(I) coordi nation of the diphosphines resulted in slight high-frequency shifts of the 31P NMR resonances of the equivalent phosphorus atoms.

Słowa kluczowe

copper(I) diphosphines perfluorinated carboxylates MS 31P NMR coordination shifts

Wydawca

Polskie Towarzystwo Chemiczne

Czasopismo

Polish Journal of Chemistry

Rocznik

2005

Tom

Vol. 79 / nr 11

Strony

1705--1711

Opis fizyczny

Bibliogr. 40 poz., rys.

Twórcy

autor

Szymańska I.

pola@chem.uni.torun.pl

Faculty of Chemistry, Nicolaus Copernicus Uni versity, 87-100 Toruń, Gagarina 7, Poland

autor

Pazderski L.

Faculty of Chemistry, Nicolaus Copernicus Uni versity, 87-100 Toruń, Gagarina 7, Poland

autor

Kucharek R.

Faculty of Chemistry, Nicolaus Copernicus Uni versity, 87-100 Toruń, Gagarina 7, Poland

autor

Szłyk E.

Faculty of Chemistry, Nicolaus Copernicus Uni versity, 87-100 Toruń, Gagarina 7, Poland

Bibliografia

1.Puddephatt R.J., J. Chem. Soc. Rev., 12,99(1983).
2.Kitagawa S., Kondo M., Kawata S., Wada S., Maekawa M. and Munakata M., Inorg. Chem., 34, 14 (1995).
3.Effendy, di Nicola C., Fianchini M., Pettinari C., Skelton B.W., Somers N. and White A.H., Inorg. Chim. Acta, 358, 763 (2005).
4.Guo L.B., Zhu J., Jiang K. and Zhang C.J., Chinese J. Inorg. Chem., 20, 1071 (2004).
5.Yang R., Hou Y., Xue B., Wang D. and Jin D„ Trans. Met. Chem, 21, 28 (1996).
6.Schmidbaur H., Bissinger P., Lachmann J. and Steigelmann O., Z. Naturforsch., B47, 1711 (1992).
7.Brandys M.C., Jennings M.C. and Puddephatt R.J., J. Chem. Soc., Dalton Trans., 24, 4601 (2000).
8.Fournier E., Lebrun F., Drouin M., Decken A. and Harvey P.D., Inorg. Chem., 43, 3127 (2004).
9.Brandys M.C. and Puddephatt R.J., Chem. Commun., 11, 1280 (2001).
10.van Calcar P.M., Olmstead M.M. and Balch A.L., Inorg. Chem., 36, 5231 (1997).
11.Brandys M.C. and Puddephatt R.J., J. Am. Chem. Soc., 123,4839 (2001).
12.Black J.R., Levason W., Spicer M.D. and Webster M., J. Chem. Soc., Dalton Trans., 20, 3129 (1993).
13.Comba P., Katsichtis C., Nuber B. and Pritzkow H., Eur. J. Inorg. Chem., 777 (1999).
14.Xie W., Wang R., Xiong Y„ Yang R., Wang D., Jin D., Chen L. and Luo B., Chinese J. Struct. Chem., 16, 293 (1997); C.A. 1997/127/170617q.
15.Yang R., Yang Y., Lin K., Wang D., Jin D., Chen J. and Li M., J. Chem., 55, 1198 (1997); C.A. 1998/128/109897k.
16.Affandi D., Bemers-Price S.J., Effendy, di Nocala C., Harvey P.J., Healy P.C., Ruch B.E. and White A.H., J. Chem. Soc.. Dalton Trans., 8, 1411 (1997).
17.Bemers-Price S.J., Johnson R.K., Mirabelli C.K, Faucette L.F., McCabe F.L. and Sadler P.J., Inorg. Chem., 26, 3383 (1987).
18.Bemers-Price S.J., Brevard C., Pagelot A. and Sadler P.J., Inorg. Client., 24, 4278 (1985).
19.Bemers-Price S.J. and Sadler P.J., Inorg. Chem., 25, 3822 (1986).
20.Szłyk E., Łakomska I. and Grodzicki A., Polish J. Chem., 68, 1529 (1994).
21.Szłyk E., Łakomska I. and Grodzicki A., Polish J. Chem., 69, 1103 (1995).
22.Łakomska I., Grodzicki A. and Szłyk E., Thermocltim. Acta, 303, 41 (1997).
23.Łakomska I., Szłyk E. and Grodzicki A., Thermochim. Acta, 315, 121 (1998).
24.Łakomska I., Grodzicki A. and Szłyk E., Polish J. Chem., 72, 492 (1998).
25.Szłyk E. and Szymańska I., Polyhedron, 18, 2941 (1999).
26.Szłyk E. and Łakomska I., Polish J. Chem., 76, 1399 (2002).
27.Szłyk E., Kucharek R. and Szymańska I., Polish J. Chem., 75, 337 (2001).
28.Szłyk E., Kucharek R. and Szymańska I., J. Coord. Chem., 53, 55 (2001).
29.Szłyk E. and Goliński A., Polish J. Chem., 74, 895 (2000).
30.Szłyk E., Szymańska I., Surdykowski A., Gtowiak T., Wojtczak A. and Goliński A., J. Chem. Soc.,Dalton Trans., 17, 3404 (2003).
31.Szłyk E., Szymańska I., Piszczek P., Goliński A. and Chaberski M., Progr. Coord, and Bioinorganic Chemistry, 6, 343 (2003).
32.Szłyk E., Kucharek R., Szymańska I. and Pazderski L., Polyhedron, 22, 3389 (2003).
33.Szłyk E., Piszczek P., Łakomska I., Grodzicki A., Szatkowski J. and Błaszczyk T., Advanced Materials Chem. Vap. Deposition, 6, 105 (2000).
34.Szłyk E., Piszczek P., Grodzicki A., Chaberski M., Goliński A., Szatkowski J. and Blaszczyk T., Advanced Materials Chem. Vap. Deposition, 7, 111 (2001).
35.Szłyk E., Piszczek P., Chaberski M. and Goliński A., Polyhedron, 20, 2853 (2001).
36.Szłyk E., Grodzicki A., Szymańska I., Wrzeszcz G. and Rozpłoch F., Polish J. Chem., 71,320 (1997).
37.Nakamoto K., Infrared Spectra of Inorganic and Coordination Compounds, 3,J edition, Wiley, New York 1978, pp. 232,333.
38.Integrated Spectral Data Base System for Organic Compounds, National Institute of Advanced Industrial Science and Technology, Tsukuba, Ibaraki, Japan; http://www.aist.go.jp/RIODB/SDBS/ (2004).
39.Yang R.N., Wang D.M., Liu Y.F. and Jin D.M., Polyhedron, 20, 585 (2001).
40.Haddad P.S., Mauro A.E. and Frem R.C.G., Quim. Nova, 24, 786 (2001).

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-article-BUJ3-0002-0186