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Abstrakty
The SEM and EDS results of coatings obtained on pure niobium and titanium alloys (NiTi and Ti6Al4V) by Plasma Electrolytic Oxidation in the electrolytes containing of 300 g and 600 g copper nitrate in 1 litre of concentrated phosphoric acid at 450 V for 3 minutes, are presented. The obtained coatings are porous and consist mainly of phosphorus within titanium and copper. For each coating, the Cu/P ratios were calculated. The maximum of that coefficient was found for niobium and Ti6Al4V alloy oxidised in the electrolyte containing 600 g of Cu(NO3)2 in 1 dm3 of H3PO4 and equaling to 0.22 (wt%) | 0.11 (at%). The minimum of Cu/P ratio was recorded for NiTi and Ti6Al4V alloys oxidised by PEO in electrolyte consisting of 300 g of copper nitrate in 1 dm3 of concentrated phosphoric acid and equals to 0.12 (wt%) | 0.06 (at%). The middle value of that ratio was recorded for NiTi and it equals to 0.16 (wt%) | 0.08 (at%).
Wydawca
Czasopismo
Rocznik
Strony
5--16
Opis fizyczny
Bibliogr. 43 poz., rys., wykr.
Twórcy
autor
- arokosz@tu.koszalin.pl
- Koszalin University of Technology, Faculty of Mechanical Engineering, Division of Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland
autor
- Tadeusz.Hryniewicz@tu.koszalin.pl
- Koszalin University of Technology, Faculty of Mechanical Engineering, Division of Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland
autor
- frsimon@ipfdd.de
- Hochschule Wismar-University of Applied Sciences Technology, Business and Design, Faculty of Engineering, DE 23966 Wismar, Germany
Bibliografia
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- 2. Hryniewicz T., On the surface treatment of metallic biomaterials (Wstęp do obróbkipowierzchniowejbiomateriałówmetalowych), 2007, ed. by Koszalin University of Technology Publishing.
- 3. Rokosz K., Electrochemical Polishing in magnetic field (Polerowanieelektrochemiczne w polumagnetycznym), 2012, ed. by Koszalin University of Technology Publishing.
- 4. Hryniewicz T., Rokicki R., Rokosz K., Co-Cr alloy corrosion behaviour after electropolishing and "magnetoelectropolishing" treatments, Surface & Coatings Technology, 62(17-18) (2008), 3073-3076.
- 5. Hryniewicz T., Rokosz K., Analysis of XPS results of AISI 316L SS electropolished and magnetoelectropolished at varying conditions, Surface & Coatings Technology, 204(16-17) (2010), 2583-2592.
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- 8. Hryniewicz T.,Rokosz K., Polarization characteristics of magnetoelectropolishing stainless steels, Materials Chemistry and Physics, 122(1) (2010),169-174.
- 9. Rokosz K., Hryniewicz T., Raaen S., Characterization of passive film formed on AISI 316L stainless steel after magnetoelectropolishing in a broad range of polarization parameters, Journal of Iron and Steel Research, 83(9) (2012), 910-918.
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- 14. Rokosz K., Hryniewicz T., Simon F., Rzadkiewicz S., Comparative XPS analysis of passive layers composition formed on AISI 304L SS after standard and high-current density electropolishing, Surface and Interface Analysis, 47(1) (2015), 87-92.
- 15. Rokosz K., Lahtinen J., Hryniewicz T., Rzadkiewicz S., XPS depth profiling analysis of passive surface layers formed on austenitic AISI 304L and AISI 316L SS after high-current-density electropolishing, Surface & Coatings Technology, 276 (2015), 516-520.
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- 20. Sowa M., Kazek-Kęsik A., Krząkała A., Socha R.P., Dercz G., Michalska J., Simka W., Modification of niobium surfaces using plasma electrolytic oxidation in silicate solutions, Journal of Solid State Electrochemistry, 18(11) (2014), 3129-3142.
- 21. Simka W., Sowa M., Socha R.P., Maciej A., Michalska J., Anodic oxidation of zirconium in silicate solutions, Electrochimica Acta, 104 (2013), 518-525.
- 22. Kazek-Kesik A., Krok-Borkowicz M., Jakobik-Kolon A., Pamula E., Simka W., Biofunctionalization of Ti-13Nb-13Zr alloy surface by plasma electrolytic oxidation. Part I, Surface & Coatings Technology, 276 (2015), 59-69.
- 23. Kazek-Kęsik A., Krok-Borkowicz M., Jakobik-Kolon A., Pamula E., Simka W., Biofunctionalization of Ti-13Nb-13Zr alloy surface by plasma electrolytic oxidation. Part II, Surface & Coatings Technology, 276 (2015), 23-30.
- 24. Simka W., Nawrat G., Chlode J., Maciej A., Winiarski A., Szade J., Radwanski K., Gazdowicz J., Electropolishing and anodic passivation of Ti6Al7Nb alloy, Przemysł Chemiczny, 90(1) (2011), 84-90.
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- 29. Rokosz K., Hryniewicz T., Raaen S., Development of plasma electrolytic oxidation for improved Ti6Al4V biomaterial surface properties, The International Journal of Advanced Manufacturing Technology, (2015), DOI: 10.1007/s00170-015-8086-y
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Uwagi
PL
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-93ff37e6-a6af-4c43-951f-87b71e528a40