The Investigation of Ground Granulated Blast Furnace Slag Geopolymer at High Temperature by Using Electron Backscatter Diffraction Analysis

• Autorzy: Aziz Ikmal Hakem , Al Bakri Abdullah Mohd Mustafa , Salleh Mohd Arif Anuar Mohd , Yoriya Sorachon , Razak Rafiza Abd , Mohamed Rosnita , Baltatu Madalina Simona

Identyfikatory

DOI

10.24425/amm.2022.137494

• Języki publikacji: EN

Abstrakty

EN

This paper elucidated the potential of electron backscatter diffraction analysis for ground granulated blast furnace slag geopolymers at 1000°C heating temperature. The specimen was prepared through the mechanical ground with sandpaper and diamond pad before polished with diamond suspension. By using advanced technique electron backscatter diffraction, the microstructure analysis and elemental distribution were mapped. The details on the crystalline minerals, including gehlenite, mayenite, tobermorite and calcite were easily traced. Moreover, the experimental Kikuchi diffraction patterns were utilized to generate a self-consistent reference for the electron backscatter diffraction pattern matching. From the electron backscatter diffraction, the locally varying crystal orientation in slag geopolymers sample of monoclinic crystal observed in hedenbergite, orthorhombic crystal in tobermorite and hexagonal crystal in calcite at 1000°C heating temperature.

Słowa kluczowe

EN

geopolymer; ground granulated blast furnace slag; electron backscatter diffraction

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2022
• Tom: Vol. 67, iss. 1
• Strony: 227--231
• Opis fizyczny: Bibliogr. 21 poz., fot., rys., tab.

Twórcy

autor

Aziz Ikmal Hakem

• Universiti Malaysia Perlis (UniMAP), Geopolymer & Green Technology, Centre of Excellence (CEGeoGTech), Perlis, Malaysia

• https://orcid.org/0000-0002-2152-8918

autor

Al Bakri Abdullah Mohd Mustafa

• Universiti Malaysia Perlis (UniMAP), Faculty of Chemical Engineering Technology, Perlis, Malaysia

• https://orcid.org/0000-0002-9779-8586

autor

Salleh Mohd Arif Anuar Mohd

• Universiti Malaysia Perlis (UniMAP), Faculty of Chemical Engineering Technology, Perlis, Malaysia

• https://orcid.org/0000-0002-9523-7558

autor

Yoriya Sorachon

• National Metal and Material Technology Center (MTEC), National Science and Technology Development Agency (NSTDA), 114, Thailand Science Park, Pahonyothin Rd., Khlong 1, KhlongLuang, PathumThani 12120, Thailand

• https://orcid.org/0000-0002-8890-5407

autor

Razak Rafiza Abd

• Department of Civil Engineering Technology, Faculty of Engineering Technology, Universiti Malaysia Perlis (UniMAP), 02100 Padang Besar, Perlis, Malaysia

• https://orcid.org/0000-0001-5499-8564

autor

Mohamed Rosnita

• Universiti Malaysia Perlis (UniMAP), Geopolymer & Green Technology, Centre of Excellence (CEGeoGTech), Perlis, Malaysia

• https://orcid.org/0000-0003-0778-9246

autor

Baltatu Madalina Simona

• Gheorghe Asachi Technical University of Iasi, Faculty of Materials Science and Engineering, 700050, Iasi, Romania

• https://orcid.org/0000-0002-5278-8958

Bibliografia

• [1] O.H. Li, L. Yun-Ming, H. Cheng-Yong, R. Bayuaji, M.M.A.B. Abdullah, F.K. Loong, T.A. Jin, N.H. Teng, M. Nabiałek, B. Jeż, N.Y. Sing, Magnetochemistry 7 (1), 9 (2021).
• [2] N. Ariffin, M.M.A.B. Abdullah, P. Postawa, S.Z.A. Rahim, M.R.R.M.A. Zainol, R.P. Jaya, A. Śliwa, M.F. Omar, J.J. Wysłocki, K. Błoch, M. Nabiałek, Materials 14, 814 (2021).
• [3] N.F. Shahedan, M.M.A.B. Abdullah, N. Mahmed, A. Kusbiantoro, S. Tammas-Williams, L.Y. Li, I.H. Aziz, P. Vizureanu, J.J. Wysłocki, K. Błoch, and M. Nabiałek, Materials 14, 809 (2021).
• [4] R. Ahmad, M.M.A.B. Abdullah, W.M.W. Ibrahim, K. Hussin, F.H. Ahmad Zaidi, J. Chaiprapa, J.J. Wysłocki, K. Błoch, M. Nabiałek, Materials 14, 1077 (2021).
• [5] M.A. Faris, M.M.A.B. Abdullah, R. Muniandy, M.F. Abu Hashim, K. Błoch, B. Jeż, S. Garus, P. Palutkiewicz, N.A. Mohd Mortar, M.F. Ghazali, Materials 14, 1310 (2021).
• [6] N. Sedira, J. Castro-Gomes, Construction and Building Materials 232, 117176 (2020).
• [7] I.H. Aziz, M.M.A.B. Abdullah, M.M. Salleh, E.A. Azimi, J. Chaiprapa, A.V. Sandu, Construction and Building Materials 250, 118720 (2020).
• [8] N.H. Jamil, M.M.A.B. Abdullah, F. Che Pa, M. Hasmaliza, W.M.A. Ibrahim, I.H.A. Aziz, B. Jeż, M. Nabiałek, Magnetochemistry 7, 32 (2021).
• [9] H. Guzmán-Carrillo, J. Pérez, M. Romero, Journal of Non Crystalline Solids. 470, 53-60 (2017).
• [10] I.H. Aziz, M.M.A.B. Abdullah, C.-Y. Heah, Y.-M. Liew, Advances in Cement Research 32 (10), 465-475 (2020).
• [11] O. Burciaga-Díaz, J.I. Escalante-García, Cement and Concrete Composites 84, 157-166 (2017).
• [12] A. Cereser, M. Strobl, S.A. Hall, A. Steuwer, R. Kiyanagi, A.S. Tremsin, E.B. Knudsen, T. Shinohara, P.K. Willendrup, A.B. da Silva Fanta, Scientific Reports 7 (1), 1-11 (2017).
• [13] A. Winkelmann, G. Cios, T. Tokarski, G. Nolze, R. Hielscher, T. Kozieł, Acta Materialia 188, 376-385 (2020).
• [14] S.I. Wright, Fundamentals of automated EBSD, in Electron backscatter diffraction in materials science2000 Springer. p. 51-64 (2000).
• [15] L. Xi, D. Gu, S. Guo, R. Wang, K. Ding, K.G. Prashanth, Journal of Materials Research and Technology 9 (3), 2611-2622 (2020).
• [16] D. D. Burduhos Nergis, P. Vizureanu, O. Corbu, Revista de Chimie 70 (4), 1262-1267 (2019).
• [16] A. Tiamiyu, V. Tari, J. Szpunar, A. Odeshi, A. Khan, International Journal of Plasticity 107, 79-99 (2018).
• [17] P. Rawn, V. Sudhakar, European Journal of Materials Science and Engineering. 04, 29-36 (2019). DOI: https://doi.org/10.36868/ejmse.2019.04.01.029.
• [18] M.M. Salleh, C. Gourlay, J. Xian, S. Belyakov, H. Yasuda, S. McDonald, K. Nogita, Scientific Reports 7 (1), 1-11 (2017).
• [19] B.T. Borkar, A.B. Borkar, D. Janardhanan, P. Deshmu, European Journal of Materials Science and Engineering 05, 03-10 (2020). DOI: https://doi.org/10.36868/ejmse.2020.05.01.003
• [20] Z. Ma, X. Tian, H. Liao, Y. Guo, F. Cheng, Journal of Cleaner Production 171, 464-481 (2018).

Uwagi

1. Błędna numeracja bibliografii.

2. The authors gratefully acknowledge the Centre of Excellence Geopolymer and Green Technology (CEGeoGTech) and the School of Materials Engineering, Universiti Malaysia Perlis (UniMAP) for their expertise and support. The authors wish to thank for the funding support obtained from the Fundamental Research Grant Scheme under the Malaysian Ministry of Education (MOE) and the support gained from “Partnership for Research in Geopolymer Concrete” in the framework of Marie Skłodowska-Curie RISE Grant Agreement (689857H2020-MSCA-RISE-2015).

3. Opracowanie rekordu ze środków MNiSW, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2024).