Analysis of chloramphenicol in drinking water using an evaporation preparative step and isotope dilution liquid chromatography–tandem mass spectrometry

• Autorzy: Li Y. , Liu X. , Zhang R. , ZomPa D. , Luo P. , Tang L. , Liu X. , Zhou Y. , Wen S.

Identyfikatory

DOI

10.1556/1326.2017.28404

• Języki publikacji: EN

Abstrakty

EN

A reliable isotope dilution method for the determination of chloramphenicol (CAP) in drinking water was developed by using an evaporation preparative step. Each sample was monitored by ultrahigh-pressure liquid chromatography (UHPLC) coupled to tandem mass spectrometry (MS/MS) using an electrospray ionization interface (ESI) in negative ion modes. Recoveries of spiked samples were in the range from 93.2% to 95.7% with intra-day relative standard deviation lower than 6.7% and inter-day relative standard deviation lower than 8.2%. Limit of quantification (LOD) was 0.002 ng/mL. The developed method was successfully applied to the analysis of CAP in drinking water of Shannan region of Tibet.

Słowa kluczowe

EN

UHPLC–MS/MS; chloramphenicol; evaporation; isotope dilution; drinking water

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2018
• Tom: Vol. 30, no. 1
• Strony: 17--20
• Opis fizyczny: Bibliogr. 31 poz., rys., tab.

Twórcy

autor

Li Y.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Liu X.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Zhang R.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

ZomPa D.

• Shannan region Centre for Disease Control and Prevention, Shannan region of Tibet, 856000, China

autor

Luo P.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Tang L.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Liu X.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Zhou Y.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Wen S.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).