Combustion synthesis process for the rapid preparation of high-purity SrO powders

• Autorzy: Granados-Correa F , Bonifacio-Martínez J

Identyfikatory

DOI

10.2478/s13536-014-0250-9

• Języki publikacji: EN

Abstrakty

EN

A rapid, safe and simple technique for the production of high purity strontium oxide powders via a chemical combustion process is reported. The combustion reactions were performed to optimize the fuel to oxidizer ratios in the reaction mixtures required to obtain pure SrO powders by varying the molar ratio of chemical precursors and the temperature. The synthesized powders were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectrometry, infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, and N2-physisorption measurements. The results indicate that crystalline SrO was obtained using a 1:1 strontium nitrate: urea molar ratio at 1000 °C after 5 minutes. In addition, high-purity, homogeneous and crystalline SrO powders were easily produced in a short time via a chemical combustion process.

Słowa kluczowe

EN

strontium oxide; chemical combustion; XRD; IR spectral analysis; thermal analysis

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2014
• Tom: Vol. 32, No. 4
• Strony: 682--687
• Opis fizyczny: Bibliogr. 23 poz., rys., wykr.

Twórcy

autor

Granados-Correa F

• Instituto Nacional de Investigaciones Nucleares, Departamento de Quımica, A.P. 18-1027. Col. Escandon, Delegacion Miguel Hidalgo. C.P. 11801 Mexico, D.F., Mexico

autor

Bonifacio-Martínez J

• Instituto Nacional de Investigaciones Nucleares, Departamento de Quımica, A.P. 18-1027. Col. Escandon, Delegacion Miguel Hidalgo. C.P. 11801 Mexico, D.F., Mexico

Bibliografia

• [1] YU J., GUO H., CHENG B., J. Solid State Chem., 179 (2006), 800.
• [2] LI S., ZHANG H., XU J., YANG D., Mater. Lett., 59 (2005),420.
• [3] YOOSUK B., KRASAE P., PUTTASAWAT B., UDOMSAP P., VIRIYA-EMPIKUL N., FAUNGNAWAKIJ K., Chem. Eng. J., 162 (2010), 58.
• [4] JOYCE A.O., Strontium, Minerals Yearbook. Volume 1. Metals and Minerals, US, Bureau of Mines, 1992, 11323.
• [5] OZUNA O., HIRATA G.A., KITTRICK M.C., J. Phys.- Condens. Mat., 16 (2004), 2585.
• [6] CHANDRAPPA K.G., VENKATESHA T.V., NAYANA K.O., PUNITHKUMAR M.K., Mater. Corros., 63 (2012), 445.
• [7] KINGSLEY J.J., PEDERSON L.R., Mater. Lett., 18 (1993), 89.
• [8] CHANDRAN R.G., PATIL K.C., Mater. Lett., 10 (1990), 291.
• [9] MANOHARAN S.S., PATIL K.C., J. Am. Ceram. Soc., 75 (1992), 1012.
• [10] LI F., HU, J. L., ZHANG L.D., CHEN G., J. Nucl. Mater., 300 (2002), 82.
• [11] PATIL K.C., ARUNA S.T., MIMAMI T., Curr. Opin. Solid St. M., 6 (6) (2002), 507.
• [12] BIAMINO S., BADINI C., J. Eur. Ceram. Soc., 24 (2004), 3021.
• [13] CHICK L.A., PEDERSON L.R., MAUPIN G.D., BATES J.L., THOMAS L.E., EXARHOS G.H., Mater. Lett., 10 (1990), 6.
• [14] SHARMA S.K., PITALE S.S., MALIK P.M., DUBEY R.N., QURESHI M.S., OJHA S., Physica B, 405 (2010), 866.
• [15] GRANADOS-CORREA F., BONIFACIO-MART´INEZ J., LARA V.H., BOSCH P., BULBULIAN S., Appl. Surf. Sci., 254 (2008), 4688.
• [16] ALVARADO-IBARRA Y., GRANADOS-CORREA F., LARA V.H., BOSCH P., BULBULIAN S., Colloid. Surface A, 345 (2009), 135.
• [17] GRANADOS-CORREA F., JIMENEZ ´ -REYES M., Sep. Sci. Technol., 46 (2011), 2360.
• [18] MEDINE G.M., KLABUNDE K.J., ZAIKOVSKII V., J. Nanopart. Res., 4 (2002),357.
• [19] MATHEWS T., SUBASRI R., SREEDHARAN O.M., Solid State Ionics, 148 (2002), 135
• [20] CRUZ D., PFEIFFER H., BULBULIAN S., Solid State Sci., 8 (2006), 470
• [21] CAMPBELL P.F., ORTNER M.H., ANDERSON C., Anal. Chem., 33 (1961), 58
• [22] SAHU R.K., RAY A.K., DAS S.K., KAILATH A.J., PATHAK L.C., J. Mater. Res., 21 (2006), 1664
• [23] LOWELL S., Introduction to Powder Surface Area, Interscience Publishers, Toronto, Canada, 1979.