Phase Analysis and Crystallographic Orientation of High Chromium Cast Iron Grain Using EBSD Technique

• Autorzy: Siekaniec D. , Kopyciński D.
• Języki publikacji: EN

Abstrakty

EN

Grain orientation, properties, microstructure borders, and types and sizes of phases have had a major impact on the traits of modern engineering materials. Therefore, it is important to study, analyze, and (further) control the method of crystallizing alloys. One of the methods used to assess the orientation of grain growth is the EBSD technique. EBSD (Electron Backscatter Diffraction Analysis) enables us to perform quantitative analyses on the microstructure of materials (on a scale of millimetres to nanometres) in a scanning electron microscope. Using the EBSD technique can help us gain valuable information about the following properties of crystalline materials: crystal orientation, disorientation, grain boundaries, global and local texture, fractions recrystallization/deformation, stress analysis, characterization of intergranular boundaries, identification of phases, phase distribution, and so on. In this paper, we present the results of phase analysis and crystallographic orientation of the grains of high chromium cast iron via EBSD. These were preliminary studies to determine the possibility of using the EBSD technique for analyzing high chromium cast iron. Castings were produced under industrial conditions, then samples were cut out and testing using the EBSD technique. This method proved to be effective for this type of material.

Słowa kluczowe

EN

microstructure; crystal orientation; EBSD technique; high chromium cast iron; grain

• Wydawca: AGH University of Science and Technology Press
• Czasopismo: Journal of Casting & Materials Engineering
• Rocznik: 2017
• Tom: Vol. 1, no. 1
• Strony: 15--19
• Opis fizyczny: Bibliogr. 9 poz., rys., tab., wykr.

Twórcy

autor

Siekaniec D.

• AGH University of Science and Technology, Faculty of Foundry Engineering

autor

Kopyciński D.

• AGH University of Science and Technology, Faculty of Foundry Engineering

Bibliografia

• [1] Faryna M. (2012). Dyfrakcja elektronów wstecznie rozproszonych w skaningowym mikroskopie elektronowym. Kraków: Wydawnictwa AGH.
• [2] Dyfrakcja elektronów wstecznie rozproszonych. Retrieved from http://www.imim.pl/files/Wyklad%20V.pdf (accessed 07.11.2016).
• [3] Explained EBSD From data acquisition to advanced analysis. Retrieved from https://www.oxford-instruments.com/ products /microanalysis/ebsd (accessed 07.11.2016).
• [4] Phase Identification and Separation in SEM. Retrieved from https://www.oxford-instruments.com/products/microanalysis/ebsd (accessed 07.11.2016).
• [5] Kang J.S., Seol J.-B. & Park C.G. (2013). Three-dimensional characterization of bainitic microstructures in low-carbon high-strength low-alloy steel studied by electron backscatter diffraction. Material Characterisation, 79, 110–121. doi: 10.1016/j.matchar.2013.02.009
• [6] Unnikrishnana R., Idury K.S.N.S., Ismail T.P; Bhadauria A., Shekhawat S.K., Khatirkar R.K. & Sapate S.G.(2014). Effect of heat input on the microstructure, residual stresses and corrosion resistance of 304L austenitic stainless steel weldments. Material Characterisation, 93, 10–23. doi:10.1016/j.matchar. 2014.03.013
• [7] Sozańska M, Chmiela B. (2012). Ocena możliwości stosowania metody EBSD w badaniach mikrostruktury stopów tytanu. Inżynieria Materiałowa, 4, 311–314.
• [8] Maitland T. & Sitzman S. (2007). Backscattering Detector and EBSD in Nanomaterials Characterization. New York: Springer.
• [9] Kamp A. (2007). Investigation of Titanium α Plates by EBSD Analysis. Master thesis. Delft University of Technology, Delf, Netherlands.