Characterization of Nanocrystalline AlTiSiN Coatings Deposited by a LARCCAE Process

• Autorzy: Gołombek K. , Tomiczek A. E. , Pakuła D. , Matus K.

Identyfikatory

DOI

10.24425/122420

• Języki publikacji: EN

Abstrakty

EN

The paper presents the results of research studies involving the ceramic-metal tool materials with the deposited nitride coatings on the basis of aluminium, titanium and silicon. The cathodic arc evaporation with lateral rotating cathodes method was used for deposition of nanocrystalline, wear resistant nitride coatings – AlTiSiN type. Structural examinations are presented of the applied coatings and their support material made on the scanning electron microscope (SEM) and the scanning/transmission electron microscope (STEM). Chemical composition analysis as a function of the distance from the specimen surface, the so-called profile analysis, were carried out also. The structural analysis confirms that deposited multilayer coatings have dense microstructure without any visible porosity and delamination. It was found that the investigated coatings have nanocrystalline structure and consisting of fine crystallites even less than 6nm. Lattice deformations and numerous structural defects were also observed in the nanolayers. Depositing the AlTiSiN coatings results in the significant hardness increase within the range of 2252 ±256 to 2908 ±295 HV_0.01.

Słowa kluczowe

EN

AlTiSiN coatings; LARC-CAE process; structural examinations

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2018
• Tom: Vol. 63, iss. 2
• Strony: 899--906
• Opis fizyczny: Bibliogr. 24 poz., fot., rys., tab.

Twórcy

autor

Gołombek K.

• Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, Akademicka 2a Str., 44-100 Gliwice, Poland

autor

Tomiczek A. E.

• Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, Akademicka 2a Str., 44-100 Gliwice, Poland

autor

Pakuła D.

• Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, Akademicka 2a Str., 44-100 Gliwice, Poland

autor

Matus K.

• Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, Akademicka 2a Str., 44-100 Gliwice, Poland

Bibliografia

• [1] S. Zhang (Ed.), Handbook of Nanostructured Thin Films and Coatings, CRC Press, Taylor and Francis Group (2010).
• [2] B. Tlili, C. Nouveau, M. J. Walock, M. Nasri, T. Ghrib, Vacuum 86, 1048-1056 (2012).
• [3] Y. Y. Chang, C. P. Chang, D. Y. Wang, S. M. Yang, W. Wu, J. Alloys Compd. 461, 336-341 (2008).
• [4] M. Parlinska-Wojtan, A. Karimi, T. Cselle, M. Morstein, Surf. Coat. Technol. 177-178, 376-381 (2004).
• [5] L. Aihua, D. Jiannxin, C. Haibing, C. Yangyang, Z. Jun, Int. J. Refract. Met. H. 31, 82-88 (2012).
• [6] M. Stueber, H. Holleck, H. Leiste, K. Seemann, S. Ulrich, C. Ziebert, J. Alloys Compd. 483, 321-333 (2009).
• [7] K. Bobzin, N. Bagcivan, N. Goebbels, K. Yilmaz, B. R. Hoehn, K. Michaelis, M. Hochmann, Surf. Coat. Technol. 204, 1097-1101 (2009).
• [8] L. A. Dobrzański, M. Szindler, M. Pawlyta, M. M. Szindler, P. Boryło, B. Tomiczek, Open Phys. 14, 159-165 (2016).
• [9] K. Gołombek, L. A. Dobrzański, M. Soković, J. Mater. Process. Technol. 157-158 341-347 (2004).
• [10] K. Lukaszkowicz, L. A. Dobrzański, G. Kokot, P. Ostachowski, Vacuum 86, 2082-2088 (2012).
• [11] E. Torres, D. Ugues, Z. Brytan, M. Perucca, J. Phys. D: Appl. Phys. 42, 105306 (2009).
• [12] K. Gołombek, G. Matula, J. Mikuła, M. Soković, Mater. Technol. 51 (1), 163-171 (2017).
• [13] L. Aihua, D. Jiannxin, C. Haibing, Ch, Yangyang, Y. Jun, Int. J. Refract. Met. H. 31, 82-88 (2012).
• [14] C. Ducros, C. Cayron, F. Sanchette, Surf. Coat. Technol. 201, 136-142 (2006).
• [15] S. Zhang, L. Wang, Q. Wang, M. Li, Surf. Coat. Technol. 214, 160-167 (2013).
• [16] W. Y. Hoa, C. H. Hsu, C. W. Chena, D. Y. Wang, Appl. Surf. Sci. 257, 3770-3775 (2011).
• [17] S. Veprek, R. F. Zhang, M. G. J. Veprek-Heijman, S. H. Sheng, A. S. Argon, Surf. Coat. Technol. 2004, 1898-1906 (2010).
• [18] L. A. Dobrzański, K. Gołombek, J. Mater. Process. Technol. 164-165, 805-815 (2005).
• [19] J. Musil, Surf. Coat. Technol. 207, 50-65 (2012).
• [20] F. Sanchette, C. Ducros, T. Schmitt, P. Steyer, A. Billard, Surf. Coat. Technol. 205, 5444-5453 (2011).
• [21] M. G. Faga, G. Gautier, R. Calzavarini, M. Perucca, E. Aimo Boot, F. Cartasegna, L. Settineri, Wear 263, 1306-1314 (2007).
• [22] H. C. Barshilia, B. Deepthi, K. S. Rajam, Vacuum 81, 479-488 (2006).
• [23] X. Z. Ding, X. T. Zeng, Y. C. Liu, Thin Solid Films 519 (6), 1894-1900 (2011).
• [24] T. Marten, B. Alling, E. Isaev, H. Lind, F. Tasnadi, L. Hultman, I. Abrikosov, Phys. Rev. B 85, 104106 (2012).

Uwagi

EN

1. This work was supported by the Ministry of Science and Higher Education of Poland as the statutory financial grant of the Faculty of Mechanical Engineering, Silesian University of Technology.

PL

2. Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).