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In this work the microstructure analysis of composite from ZrO2 – Ti system were presented. For the preparation of the composite samples nanometric ZrO2 powder stabilized by 3 mol% of Y2O3 and micrometric titanium powder were used. The composites with 10 vol.% addition of titanium particles were prepared by slip casting method. The sintering process was conducted at 1450°C with 2 hours’ dwell time, in the inert atmosphere of argon. The microstructure observations were carried out with the use of SEM and STEM microscopes. The quantitative analysis and stereological characterization were performed. The SEM and STEM observations allowed characterizing the microstructure of composite samples. Especially, the interface between titanium particles and zirconia matrix was described. The growth of the zirconia grains around the Ti rich areas was observed. The increase of the zirconia grains size results from the reaction on the interface between titanium particle and zirconia matrix during the sintering process.
Słowa kluczowe
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Czasopismo
Rocznik
Tom
Strony
2045--2049
Opis fizyczny
Bibliogr. 15 poz., rys., wykr.
Twórcy
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, 141 Woloska Str., Warszawa, Poland
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, 141 Woloska Str., Warszawa, Poland
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, 141 Woloska Str., Warszawa, Poland
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, 141 Woloska Str., Warszawa, Poland
Bibliografia
- [1] J. Kapuściński, Kompozyty: podstawy projektowania i wytwarzania, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa 1993.
- [2] A. Boczkowska, Kompozyty, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa 2003.
- [3] E. Fernandes-Garcia, C. F. Gutierrez-Gonzalez, P. Peretyagin, W. Solis, S. Lopez-Esteban, R. Torrecillas, A. Fernandez, Effect of yttria-titanium shell-core structured powder on strength and ageing of zirconia/titanium composites, Mater. Sci. Eng. A 646, 96-100 (2015).
- [4] K. Tohgo, T. Fujii, M. Harada, H. Isono, Y. Shimamura, Fabrication of PSZ-Ti composites by spark plasma sintering and their mechanical properties, Mate.r Sci. Eng. A 621, 166-172 (2015).
- [5] T. Yoshida, T. Hoshima, I. Mkaizawa, S. Sakurada, Properties of partially stabilized zirconia fuel cell, J. Electrochem. Soc. 136 (1989).
- [6] M. A. Borik, V. T. Bublik, A. V. Kulebyakin, E. E. Lomonova, F. O. Milovich, V. A. Myzina, V. V. Osiko, N. Y. Tabachkova, Phase composition, structure and mechanical properties of PSZ (partially stabilized zirconia) crystals as a function of stabilizing impurity content, J. Alloy Compd. 586, 231-235 (2014).
- [7] M. Niinomi, Mechanical properties of biomedical titanium alloys, Materials Science and Engineering A 243, 231-236 (1998).
- [8] R. Ruh, Reaction of zirconia and titanium at elevated temperatures, J. Am. Ceram. Soc. 46, 301-306 (1963).
- [9] B. C. Weber, H. J. Garrett, F. A. Mauer, M. A. Schwartz, Observations on the stabilization of zirconia”, J. Am. Ceram. Soc. 39 (1956).
- [10] R. Ruh, N. M. Tallan, H. A. Lipsitt, Effect of metal additions on the microstructure of zirconia”, J. Am. Ceram. Soc. 47, 632-635 (1964).
- [11] K. L. Lin, C. C. Lin, Ti2ZrO Phases formed in the titanium and zirconia interface after reaction at 1550°C, J. Am. Ceram. Soc. 88, 1268-1272 (2005).
- [12] K. L. Lin, C. C. Lin, Zirconia-related phases in the zirconia/titanium diffusion couple after annealing at 1100-1550°C, J. Am. Ceram. Soc. 88, 2928-2934 (2005).
- [13] K. L. Lin, C. C. Lin, Effected of annealing temperature on microstructural development at the interface between zirconia and titanium, Journal of the American Ceramic Society 90, 893-899 (2007).
- [14] M. Chmielewski, S. Nosewicz, D. Jakubowska, M. Lewandowska, J. Mizera, J. Rojek, P. Bazarnik, The influence of sintering time on the microstructural properties of chromium-rhenium matrix composites, Int. J. Refract. Met. H 59, 78-86 (2016).
- [15] T. Wejrzanowski, R. Pielaszek, A. Opalińska, H. Matysiak, W. Łojkowski, K. J. Kurzydłowski, Quantitative methods for nanopowders characterization, Appl. Surf. Sci. 253, 204-208 (2006).
Uwagi
EN
The work was done in frame of the project financed by National Center of Science (NCN), project DEC-2013/11/B/ ST8/00309
PL
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-f7cf3f52-0d61-4e40-bf2b-48bd55c2d649