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Determination of Alphacypermethrin in the Air by Capillary Gas Chromatography

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Treść / Zawartość
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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A new method for sampling and chemical analysis of alphacypermethrin in workplace air has been described. Air samples were taken using a glass tube filled with silica gel with chemically bounded octadecyl phase. Chromatographic determinations were conducted using an HP-5 capillary column (10 m x 0.53 mm) and an electron-capture detector. Alphacypermethrin recovery was 100.15%. The calculated detection limit for a 60-L air sample was 0.0001 mg/m3.
Rocznik
Strony
529--536
Opis fizyczny
Bibliogr. 12 poz., tab., wykr.
Twórcy
autor
  • W. Chodzko Institute of Agricultural Medicine, Poland
Bibliografia
  • [1] Bottomley, P., & Baker, P.G. (1984). Multi-residue determination of organochlorine, organophosphorous and synthetic pyrethroid pesticides in grain by gas-liquid and high performance liquid chromatography. Analyst, 109, 85-109.
  • [2] Chapman, R.A. (1983). Chiral-phase high-performance liquid chromatographic separation of enantiomers of pyrethroids insecticide esters derived from α-cyano-3 phenoxybenzyl alcohol. Journal of Chromatography, 258, 175-182.
  • [3] Ludwicki, J.K., Góralczyk, K., & Czaja, K. (1989). Determination of insecticides from synthetic pyrethroids group in plant material. Roczniki PZH , XXXIX, 302-307. (In Polish).
  • [4] Nakamura, Y., Tonogai, Y., Sekiguchi, Y., Tsumura, Y., Nischida, N., Takakura, K., Isechi, M., Yuasa, K., Nakanura, M., Kifune, N., Yamamoto, K., Teresawa, S., Oshima, T., Miyata, M., Kamakura, K., & Ito, Y. (1994). Multiresidue analysis of 48 pesticides in agricultural products by capillary gas chromatography. Journal of Agriculture and Food Chemistry, 42, 2508-2518.
  • [5] Nehmer, U., & Dimov, N. (1994). High performance liquid chromatographic determination of kadethrin, permethrin and piperonyl butoxide in spray solutions. Journal of Chromatography, 288, 227-229.
  • [6] Papadopoulu-Mourkidou, E. (1988). Recent advances in pyrethroid determination. In J. Sherma (Ed.), Analytical methods for pesticides and plant growth regulators (Vol. XVI, pp. 179-203). San Diego, CA, USA: Academic Press.
  • [7] Perkow, W. (1985). Wirksubstanzen der Phlanzenschutz- und Schandlings bekampfungsmitlel [Effective substances for plant protection and pesticides control]. Berlin, Germany: Paul Parey.
  • [8] Pomorska, K. (1993a). Determination of deltamethrine aerosols in the air by gas chromatography. Chemia Analityczna, 38, 157-160.
  • [9] Pomorska, K. (1993b) Development of standards for determination of pesticides in the air. Postdoctoral dissertation. Lublin, Poland: Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej. (In Polish).
  • [10] Suprynowicz, Z., Buszewski, B., & Pomorska, K. (1981). New kinds of sorbents for taking pesticide samples form the air. Sorbents with chemically bonded phase. Polish Journal o f Chemistry, 55(10), 2123-2127.
  • [11] Walters, S.M. (1983). Preliminary evaluation of high-performance liquid chromatography with photoconductivity detection for the determination of selected pesticides as potential food contaminants. Journal of Chromatography, 259, 224-227.
  • [12] Worthing, C.R. (Ed.). (1991). The pesticide manual. A world compendium. London, UK: The British Crop Protection Council.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-f5e13c1c-831a-4bfc-89fc-55e4ec40849f
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