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EDS technique appliance for investigation of laser remelted and alloyed magnesium cast alloys

Wybrane pełne teksty z tego czasopisma
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: The paper presents the results of the qualitative and quantitative microanalysis of the chemical composition of the MgAl6Zn1 alloy. Design/methodology/approach: The magnesium alloy has been heat treatment at 505°C for 600 min and ageing at 170°C for 720 min. The study was performed on a transmission electron microscope FEI TITAN company operating at 300kV operating voltage. The qualitative and quantitative microanalysis of the chemical composition of the Mg alloy microareas was examined using EDS. Findings: Analysis of the results of the concentration of the main alloying elements in the separation test using various magnifications revealed that with an increase in the share of the magnification of the alloying elements. This increase is referred to a linear, the regression coefficient R2, depending on the test element is in the range 0.84-0.97. Practical implications: Tested MgAl6Zn1 alloy can be applied among the others in automotive industry but it requires additional researches. Originality/value: It was demonstrated that the lower magnesium concentration in the EDS results is connected with the increase of magnification induces an effect of X-rays scattering only from the analysed particles and the effect of Mg matrix is limited.
Rocznik
Strony
59--63
Opis fizyczny
Bibliogr. 17 poz., rys., tab.
Twórcy
autor
  • Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
autor
  • Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
  • Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
  • Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
Bibliografia
  • [1] A. Barbacki, Electron microscopy, Publisher of the Poznan University of Technology, Poznań 2003 (in Polish).
  • [2] L. Błaż, J. Kaneko, M. Sugamata, Microstructural evolution in mechanically alloyed Al- heavy metal oxide composites, Materials Chemistry and Physics (2003) 387-389.
  • [3] L.A. Dobrzański, E. Hajduczek, Light and electron microscopy, WNT Publisher, Warszawa 1987 (in Polish).
  • [4] A. Laskin, J.P. Cowin, M.J. Iedema, Analysis of individual environmental particles using modern methods of electron microscopy and X-ray microanalysis, Journal of Electron Spectroscopy 150/2-3 (2006) 260-274.
  • [5] H. Kaczmarek, R. Czajka, M. Nowicka, M. Wiśniewski, Polymers investigation using AFM microscope, Polymers 48/2 (2003) 91-98 (in Polish).
  • [6] D.A. Wollman, K.D. Irwin, G.C. Hilton, L.L. Dulcie, D.E. Newbury, J.M. Martinis, High-resolution, energy-dispersive microcalorimeter spectrometer for X-ray microanalysis, Journal of Microscopy 188/3 (1997) 196-223.
  • [7] B. Fultz, J.M. Howe, Transmission electron microscopy and diffractometry of Materials, SpringerVerlag Heildelberg, 2001.
  • [8] J. Goldstein, D.E. Newbury, D.C. Joy, C.E. Lyman, P. Echlin, E. Lifshin, L. Sawyer, Scanning electron microscopy and X-ray microanalysis, Kluwer Academic/Plenum Publishers, New York, 2003.
  • [9] D.B. Wiliams, C.B. Carter, Transmission electron microscopy, Plenum Press, New York, 1996.
  • [10] A. Stanisz, Statistic basic for researcher issue 21 correlation analysis, Practical Medicine 10 (2000) 176-181 (in Polish).
  • [11] I. Dziubiński, T. Świątkowski, Methematic guaid, PWN Publisher, Warszawa, 1980 (in Polish).
  • [12] W. Ozgowicz, K. Labisz, Analysis of the state of the fine-dispersive precipitations in the structure of high strength steel Weldox 1300 by means of electron diffraction, The Journal of Iron and Steel Research 18/1 (2011) 135-142.
  • [13] T. Tański, K. Labisz, Electron microscope investigation of PVD coated aluminium alloy surface layer, Solid State Phenomena 186 (2012) 192-197.
  • [14] J. Konieczny, L.A Dobrzański, K. Labisz, J. Duszczyk, The influence of cast method and anodizing parameters on structure and layer thickness of aluminium alloys, Journal of Matererials Processing and Technology 157-158 (2004) 718-723.
  • [15] A. Włodarczyk-Fligier, L.A. Dobrzanski, J. Konieczny, Structure of EN AW-Al Cu4Mg1 (A) composite materials reinforced with the Ti (C, N) ceramic particles, Journal of Achievements in Materials and Manufacturing Engineering 51/1 (2012) 22-29.
  • [16] M. Adamiak, Microstructural characterisation of EN AW6061 alloy matrix composites with Ti3Al intermetallics reinforcement, Journal of Achievements in Materials and Manufacturing Engineering 31/2 (2008) 290-293.
  • [17] L.A. Dobrzański, M. Krupiński, K. Labisz, B. Krupińska, A Grajcar, Phases and Structure Characteristics of the Near Eutectic Al-Sl-Cu Alloy Using Derivative Thermo Analysis, Materials Science Forum 638-642 (2010) 475-480.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-f39d02c6-b662-4c2f-8748-c1e0130037af
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