Preparation and characterisation of Pd nanocatalyst supported on nickel mesh

• Autorzy: Tomiczek B. , Szindler Marek , Łukowiec D. , Pawlyta M. , Nuckowski P. , Lukaszkowicz K. , Krzywiecki M. , Kříž A. , Basiaga M. , Polański J.

Identyfikatory

DOI

10.5604/01.3001.0054.2997

• Języki publikacji: EN

Abstrakty

EN

The primary aim of the publication is to show the possibility of the synthesis of palladium nanoparticles directly on the nickel molecular mesh. A combination of chemical and physicochemical methods was used. Design/methodology/approach Palladium chloride was chosen as the precursor of palladium nanoparticles, dissolved in alcohol, water or a mixture thereof. Surface topography studies of the prepared nanoparticles were made using a scanning electron microscope, Supra 35 (Zeiss’s company), and transmission electron microscope S/TEM TITAN 80-300 (FEI company). Qualitative studies were performed using spectroscopy of scattered X-ray energy using the Energy Dispersive Spectrometer to define the chemical composition of prepared nanocatalysts. The chemical states of the elements were analysed using X-ray photoelectron spectroscopy. Nanocatalyst structures were identified using X-ray crystallography. Findings Using such methods proved that the obtained material is Pd-Ni synthesised using a mixture of alcohol and water assisted by ultrasound. Nanoparticles with oval shapes and diameters below 10 nm were obtained. Research limitations/implications During the tests, it was decided to abandon the use of the ascorbic acid reducer, which, combined with the temperature, had a negative impact on the nickel substrate. Practical implications Nanocatalyst has been achieving a gradually increasing interest from researchers in environmental areas. The developed materials can be used in low-temperature carbon dioxide methanation. Originality/value The results provide a novel road for designing and developing efficient, low-cost, and low-temperature double metallic catalysts.

Słowa kluczowe

EN

nanotechnology; nanoparticles; nanocatalyst; renewable energy; methanation

PL

nanotechnologia; nanocząsteczki; nanokatalizator; energia odnawialna; metanizacja

• Wydawca: International OCSCO World Press
• Czasopismo: Journal of Achievements in Materials and Manufacturing Engineering
• Rocznik: 2023
• Tom: Vol. 121, nr 2
• Strony: 212--220
• Opis fizyczny: Bibliogr. 20 poz., rys., tab., wykr.

Twórcy

autor

Tomiczek B.

• Scientific and Didactic Laboratory of Nanotechnology and Material Technologies, Faculty of Mechanical Engineering, Silesian University of Technology, ul. Towarowa 7, 44-100 Gliwice, Poland

autor

Szindler Marek

• Scientific and Didactic Laboratory of Nanotechnology and Material Technologies, Faculty of Mechanical Engineering, Silesian University of Technology, ul. Towarowa 7, 44-100 Gliwice, Poland

• https://orcid.org/0000-0001-9938-4646

autor

Łukowiec D.

• Materials Research Laboratory, Faculty of Mechanical Engineering, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland

autor

Pawlyta M.

• Materials Research Laboratory, Faculty of Mechanical Engineering, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland

autor

Nuckowski P.

• Materials Research Laboratory, Faculty of Mechanical Engineering, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland

autor

Lukaszkowicz K.

• Department of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland

autor

Krzywiecki M.

• Centre for Science and Education, Institute of Physics, Silesian University of Technology, ul. Konarskiego 22b, 44-100 Gliwice, Poland

autor

Kříž A.

• Institute of Technology and Materials, Faculty of Mechanical Engineering, Jan Evangelista Purkyne University in Ústí nad Labem, 1 Pasteurova Str., 400 96 Ústí nad Labem, Czech Republic

autor

Basiaga M.

• Department of Biomaterials and Medical Devices Engineering, Faculty of Biomedical Engineering, Silesian University of Technology, ul. Roosevelta 40, 41-800 Zabrze, Poland

autor

Polański J.

• Centre for Materials and Drug Discovery, Institute of Chemistry, Faculty of Science and Technology, University of Silesia, ul. Szkolna 9, 40-006 Katowice, Poland

Bibliografia

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