Analysis of the Influence of an XY Electronic Mechanism with UV-Vis Spectroscopy on the Production of Gold Nanoparticles by Laser Ablation for Applications in Environmental Nanosensing

• Autorzy: Carbajal-Morán Hipólito , Márquez-Camarena Javier F. , Ingaruca-Álvarez Ever F. , Zárate-Quiñones Rosa H.

Identyfikatory

DOI

10.12911/22998993/165896

• Języki publikacji: EN

Abstrakty

EN

The work consisted in analyzing the influence of an electronic positioning mechanism of an Au metal plate in the XY axes; to optimize the production of Au metal nanoparticles by laser ablation in sterile water samples as well as to obtain morphology and size required for environmental nanosensors. The positioning mechanism is constituted by two M35SP stepper motors of 5 V DC with a rotation angle of 7.5° per step; the one that generates the displacement for each axis of XY coordinates, controlled by an algorithm implemented in Arduino Nano ATmega328, being the driver of the stepper motors the H-bridge of the L298N module, with which it was possible to set the speed to 2 mm/s, which enabled to make the wear of the metal plate uniform in the process of generation of gold nanoparticles (AuNPs). With the pulsed laser generator with ablation frequency of 10 Hz and wavelengths of 532 nm and 1064 nm, the Au metal plate was irradiated for 10 min, 20 min and 30 min. AuNPs were generated in colloidal state both for the process with fixed position of the metal plate and for the process using the electronic mechanism of XY positioning; they were characterized by UV-Vis spectroscopy with range from 300 nm to 850 nm. It was found that the production of AuNPs with the Au plates mobilized by the mechanism under study, generates colloids of spherical AuNPs of smaller diameter, close to 10 nm, with an average reduction of 19% in relation to that generated with the fixed position plate; likewise, the concentration of the AuNPs increased by 20.40%; therefore, the influence of the XY positioning electronic mechanism was positive in the production of AuNPs with morphology and sizes suitable for use in environmental nanosensors.

Słowa kluczowe

EN

XY displacement; nanoparticles; step motor control; UV-Vis spectroscopy; nanosensor

• Wydawca: Polskie Towarzystwo Inżynierii Ekologicznej ; Lublin University of Technology
• Czasopismo: Journal of Ecological Engineering
• Rocznik: 2023
• Tom: Vol. 24, nr 8
• Strony: 52--61
• Opis fizyczny: Bibliogr. 25 poz., rys., tab.

Twórcy

autor

Carbajal-Morán Hipólito

• Instituto de Investigación de Ciencias de Ingeniería, Facultad de Ingeniería Electrónica-Sistemas, Universidad Nacional de Huancavelica, Jr. La Mar 755, Pampas 09156, Huancavelica, Perú

• https://orcid.org/0000-0002-1661-5363

autor

Márquez-Camarena Javier F.

• Instituto de Investigación de Ciencias de Ingeniería, Facultad de Ingeniería Electrónica-Sistemas, Universidad Nacional de Huancavelica, Jr. La Mar 755, Pampas 09156, Huancavelica, Perú

• https://orcid.org/0000-0002-0523-9569

autor

Ingaruca-Álvarez Ever F.

• Facultad de Ingeniería Química, Universidad Nacional del Centro del Perú, Av. Mariscal Castilla N° 3909-4089, Huancayo 12006, Junín, Perú

• https://orcid.org/0000-0003-4142-4507

autor

Zárate-Quiñones Rosa H.

• 3 Facultad de Ciencias Forestales y del Ambiente, Universidad Nacional del Centro del Perú, Av. Mariscal Castilla N° 3909-4089, Huancayo 12006, Junín, Perú

• https://orcid.org/0000-0002-6553-0585

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