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Effect of grain size and tungsten addition on microstructure and magnetic properties of Nd-Fe-B type magnets

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: The paper presents the results of the microstructural and magnetic examinations of Nd-Fe-B type magnets produced by the mechanical powder milling method and doped with tungsten. Design/methodology/approach: The effect of the grain size and addition of tungsten on the microstructure and magnetic properties of nanocrystalline alloys of the basic composition of Nd10Fe84B6, as produced by the method of mechanical alloying in the process of prolonged milling, was investigated in the study. Powders were subjected to milling for a duration ranging from 10 to 120 hours in an Ar protective atmosphere. Moreover tungsten was added to the base alloy that exhibited the best magnetic parameters. The tungsten content of alloys varied in a broad range from 0 to 33 at%. Findings: The examinations have shown that the grinding duration, for which the best magnetic properties are obtained, is 90 hours. Prolonged grinding has a significant effect on the grain size and microstructure refinement. The alloy addition in the form of tungsten, similarly as in the case of prolonged grinding, leads to a structure refinement. In the case of W addition, an increase in the coercive field, with a simultaneous decrease in the value of remanence and magnetic energy density (BH)max, is observed. Practical implications: Development of relatively cheap Nd10Fe84B6 magnets of good service properties. Originality/value: Determination of the effect of grain size and tungsten content on the magnetic properties and microstructure of the Nd-Fe-B magnets.
Słowa kluczowe
Rocznik
Strony
210--214
Opis fizyczny
Bibliogr. 12 poz., rys.
Twórcy
autor
  • Institute of Physics, Faculty of Materials Processing Technology and Applied Physics, Częstochowa University of Technology
autor
  • Institute of Physics, Faculty of Materials Processing Technology and Applied Physics, Częstochowa University of Technology
autor
  • Institute of Physics, Faculty of Materials Processing Technology and Applied Physics, Częstochowa University of Technology
  • Institute of Physics, Faculty of Materials Processing Technology and Applied Physics, Częstochowa University of Technology
Bibliografia
  • [1] M. Sagawa, S. Fujimura, M. Togawa, H. Yamamoto, Y. Matsuura, New material for permanent magnets on a base of Nd and Fe, Journal of Applied Physics 55/6 (1984) 2083-2087.
  • [2] J.J. Croat, J.F. Herbst, R.W. Lee, F.E. Pinkerton, Pr-Fe and Nd-Fe based materials: A new class of high - performance permanent magnets, Journal of Applied Physics 55/6 (1984) 2078-2082.
  • [3] H. Kronmüller, T. Schrefl, Interactive and cooperative magnetization processes in hard magnetic materials, Journal of Magnetism and Magnetic Materials 129/1 (1994) 66-78.
  • [4] K. H. J. Bushow, New permanent magnets, Materials Science Reports 1/1 (1986) 1-63.
  • [5] H. Bala, S. Szymura, J.J. Wysłocki, Electrochemical corrosion resistance of Fe-Nd-B permanent magnets, Journal of Materials Science 25/1 (1990) 571-574.
  • [6] M. Leonowicz, J.J. Wysłocki, Modern magnets, WNT, Warsaw, 2005, 72-92 (in Polish).
  • [7] P.J. McGuiness, C. Short, A.F. Wilson, I.R. Harris, The production and characterization of bonded, hot-pressed and die-upset HDDR magnets, Journal of Alloys and Compounds 184/2 (1992) 243-255.
  • [8] J.J. Wyslocki, P. Pawlik, Arc-plasma spraying and suction- custing metods in magnetic materials manufacturing, Journal of Achievements in Materials and Manufacturing Engineering 43/1 (2010) 463-468.
  • [9] H.H. Stadelmaier, E.T. Henig, G. Petzof, A chronic of development of iron based rare earth high-performence magnets, Zeitschrift für Mettallkunde 82/3 (1991) 163-168.
  • [10] E. Girt, Z. Altounian, D.H. Ryan, Fe-substitution in Nd2Fe17-δXδC0,3 (X = Al, Ti, V, W and δ = 0, 0.5), Journal of Magnetism and Magnetic Materials 177-181/2 (1998) 982-984.
  • [11] A. Yan, X. Song, X. Wang, Segregation of W in Nd-Fe-B magnets and its effect on coercivity, IEEE Transactions on Magnetics. 36/4 (2000) 2033-2036.
  • [12] A. Przybył, J.J. Wysłocki, The effect of annealing temperature on structure and magnetic properties of nanocomposite Nd10Fe84-xWxB6 (0
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-ed90eef4-27aa-4669-bae4-655a3160fbad
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