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Języki publikacji
Abstrakty
Metaldehyde is a molluscicide allowed for use in the control of slugs and snails in agriculture and horticulture in many countries. A simple, fast, and precise gas chromatography method was developed and single-laboratory validated for determination of metaldehyde in different formulations of plant protection products. The proposed method involves extraction of active substance from samples by sonication with acetone and analysis using gas chromatography–flame ionization detection (GC–FID). The suggested analytical procedure is accurate, precise, and repeatable. Moreover, it is environmentally friendly and useful for laboratories as it uses a no time- and no solvent-consuming reference chromatography technique for quality control of commercially available pesticide formulations. Advantages of the proposed method are consistent with the ideas of sustainable development, which are in accordance with the principles of Green Analytical Chemistry. Analysis of real samples of commercial pesticide formulations confirmed that the proposed method is fit for its purpose.
Czasopismo
Rocznik
Tom
Strony
286--290
Opis fizyczny
Bibliogr. 29 poz., rys., tab.
Twórcy
autor
- Pesticide Quality Testing Laboratory, Institute of Plant Protection—National Research Institute Sośnicowice Branch, Gliwicka 29, 44-153 Sośnicowice, Poland
autor
- Pesticide Quality Testing Laboratory, Institute of Plant Protection—National Research Institute Sośnicowice Branch, Gliwicka 29, 44-153 Sośnicowice, Poland
autor
- Pesticide Quality Testing Laboratory, Institute of Plant Protection—National Research Institute Sośnicowice Branch, Gliwicka 29, 44-153 Sośnicowice, Poland
- Department of General Chemistry and Chromatography, Institute of Chemistry, University of Silesia, Szkolna 9, 40-006 Katowice, Poland
autor
- Department of General Chemistry and Chromatography, Institute of Chemistry, University of Silesia, Szkolna 9, 40-006 Katowice, Poland
Bibliografia
- [1] MacBean C. A World Compendium, The Pesticide Manual; 16th edn. BCPC: Alton; 2012.
- [2] EU Pesticides database, http://ec.europa.eu/food/plant/pesticides/eu-pesticides-database/public/?event=homepage&language=EN (accessed May 2018).
- [3] Institute of Plant Protection – National Research Institute, Zalecenia ochrony roślin. Część I. Wykaz środków ochrony roślin; Institute of Plant Protection– National Research Institute: Poznań; 2004–2017.
- [4] Ministry of Agriculture and Rural Development, https://bip.minrol.gov.pl/Informacje-Branzowe/Produkcja-Roslinna/Ochrona-Roslin/Rejestr-Srodkow-Ochrony-Roslin (accessed May 2018).
- [5] Bundesamt für Verbraucherschutz und Lebensmittelsicherheit, https://apps2.bvl.bund.de/psm/jsp/index.jsp?modul=form (accessed May 2018).
- [6] Pesticides Register of UK, Health and Safety Executive. Plant Protection Products with Authorisation for use in the UK, https://secure.pesticides.gov.uk/pestreg/ProdSearch.asp (accessed May 2018).
- [7] Booze, T. F.; Oehme, F. W. J. Anal. Toxicol. 1985, 9, 172–173.
- [8] Iwata, Y.; Carman, G. E.; Dinoff, T. M.; Gunther, F. A. J. Agric. Food Chem. 1982, 30, 606–608.
- [9] Zhang, X. Y.; Dai, X. F. Chin. J. Pest. Science 2006, 8, 344–348.
- [10] Coloso, R. M.; Borlongan, I. G.; Blum, R. A. Crop Protect 1998, 17, 669–674.
- [11] Zhang, Z.; Lefebvre, T.; Kerr, C.; Osprey, M. J. Sep. Science 2014, 37, 3699–3705.
- [12] Jones, A.; Charlton, A. J. Agric. Food Chem. 1999, 47, 4675–4677.
- [13] Zhang, H.; Wang, C.; Lu, H.; Guan, W.; Ma, Y. Ecotoxicol. Environ. Saf. 2011, 74, 1653–1658.
- [14] Dong, B.; Shao, X.; Lin, H.; Hu, J. Food Chem. 2017, 229, 604–609.
- [15] Ma, Y. Q.; Wu, X. L.; Zheng, Z. T.; Yang, Y.; Wang, C.; Zhang, H. Y.; Meng, L. X. Adv. Mater. Res. 2012, 347–353, 1987–1993.
- [16] Zang, H. Y.; Wang, C.; Xu, P. J.; Ma, Y. Q. Food Addit. Contam. Part A 2011, 28, 1034–1040.
- [17] Li, C.; Wu, Y. L.; Yang, T.; Zhang, Y. Chromatographia 2010, 72, 987–991.
- [18] Schumacher, M.; Castle, G.; Gravell, A.; Mills, G. A.; Fones, G. R. MethodsX 2016, 3, 188–194.
- [19] Li, X.; Peng, T.; Jia, R.; Chen, D.; Dai, H. Food Science 2011, 32, 224–228.
- [20] Saito, T.; Morita, S.; Motojyuku, M.; Akieda, K.; Otsuka, H.; Yamamoto, I.; Inokuchi, S. J. Chromatogr. B 2008, 875, 573–576.
- [21] Selim, S.; Seiber, J. N. J. Agric. Food Chem. 1973, 21, 430–433.
- [22] American Chemical Society, 12 Principles of Green Chemistry, https://www.acs.org/content/acs/en/greenchemistry/what-is-green-chemistry/principles/12-principles-of-green-chemistry.html (accessed May 2018).
- [23] Tobiszewski, M.; Mechlińska, A.; Namieśnik, J. Chem. Soc. Rev. 2010, 39, 2869–2878.
- [24] Namieśnik J. J. Sep. Science 2001, 24, 151–153.
- [25] Tobiszewski, M.; Namieœnik, J. Trends Anal. Chem. 2012, 35, 67–73.
- [26] European Commission, Regulation (EC) No 1107/2009 of the European Parliament and of the Council of 21 October 2009 concerning the placing of plant protection products on the market and repealing Council Directives 79/117/EEC and 91/414/EEC), http://eur-lex.europa.eu/legal-content/EN/TXT/PDF/?uri=CELEX:32009R1107&from=EN (accessed May 2018).
- [27] Directorate General Health and Consumer Protection, SANCO/3030/99 rev. 4. Technical Material and Preparations, https://ec.europa.eu/food/sites/food/files/plant/docs/pesticides_ppp_app-proc_guide_phys-chem-ana_tech-mat-preps.pdf (accessed May 2018).
- [28] Collaborative International Pesticide Analytical Council, Guidelines on method validation to be performed in support of analytical methods for agrochemical formulations, http://cipac.org/images/pdf/validat.pdf (accessed May 2018).
- [29] Collaborative International Pesticide Analytical Council, Guidelines for analytical methods for the determination of relevant impurities referred to in FAO and/or WHO specifications for pesticide technical grade active ingredients and formulations, http://cipac.org/images/pdf/CIPAC_Guideline%20Relevant%20impurities_June%202009.pdf (accessed May 2018).
Uwagi
PL
Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-ea92b349-8bbd-4a17-8eec-f9dc316e21dd