A review of micro-solid-phase extraction techniques and devices applied in sample pretreatment coupled with chromatographic analysis

Dugheri, Stefano; Marrubini, Giorgio; Mucci, Nicola; Cappelli, Giovanni; Bonari, Alessandro; Pompilio, Ilenia; Trevisani, Lucia; Arcangeli, Giulio

doi:10.1556/1326.2020.00790

Artykuł - szczegóły

Tytuł artykułu

A review of micro-solid-phase extraction techniques and devices applied in sample pretreatment coupled with chromatographic analysis

Autorzy

Dugheri Stefano , Marrubini Giorgio , Mucci Nicola , Cappelli Giovanni , Bonari Alessandro , Pompilio Ilenia , Trevisani Lucia , Arcangeli Giulio

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.1556/1326.2020.00790

Warianty tytułu

Języki publikacji

Abstrakty

Sample pretreatment is one of the most crucial and error-prone steps of an analytical procedure; it consents to improve selectivity and sensitivity by sample clean-up and pre-concentration. Nowadays, the arousing interest in greener and sustainable analytical chemistry has increased the development of microextraction techniques as alternative sample preparation procedures. In this review, we aimed to show two different categorizations of the most used micro-solid-phase extraction (mSPE) techniques. In essence, the first one concerns the solid-phase extraction (SPE) sorbent selection and structure: normalphase, reversed-phase, ion-exchange, mixed-mode, molecular imprinted polymer, and special techniques (e.g., doped cartridges for specific analytes). The second is a grouping of the commercially available mSPE products in categories and sub-categories. We present every device and technology into the classifications paying attention to their historical development and the actual state of the art. So, this study aims to provide the state-of-the-art of mSPE techniques, highlighting their advantages, disadvantages, and possible future developments in sample pretreatment.

Słowa kluczowe

micro-solid-phase extraction solid-phase extraction liquid chromatography gas chromatography sample pretreatment sample purification

Wydawca

University of Silesia in Katowice
Akademiai Kiado

Czasopismo

Acta Chromatographica

Rocznik

2021

Tom

Vol. 33, no. 2

Strony

99--111

Opis fizyczny

Bibliogr. 89 poz., rys., tab.

Twórcy

autor

Dugheri Stefano

stefano.dugheri@unifi.it

Industrial Hygiene and Toxicology Laboratory, Careggi University Hospital, Florence, Italy

https://orcid.org/0000-0002-3078-7188

autor

Marrubini Giorgio

Department of Drug Sciences, University of Pavia, Pavia, Italy

autor

Mucci Nicola

Department of Experimental and Clinical Medicine, University of Florence, Florence, Italy

autor

Cappelli Giovanni

Department of Experimental and Clinical Medicine, University of Florence, Florence, Italy

autor

Bonari Alessandro

General Laboratory, Careggi University Hospital, Florence, Italy

autor

Pompilio Ilenia

General Laboratory, Careggi University Hospital, Florence, Italy

autor

Trevisani Lucia

Department of Experimental and Clinical Medicine, University of Florence, Florence, Italy

autor

Arcangeli Giulio

Department of Experimental and Clinical Medicine, University of Florence, Florence, Italy

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Uwagi

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).

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Bibliografia

Identyfikator YADDA

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