The Application of the Mechanochemical Synthesis for the Preparation of Advanced Ceramics Based on Barium Titanate

• Autorzy: Garbarz-Glos B. , Bąk W. , Budziak A. , Dulian P. , Lisińska-Czekaj A. , Czekaj D.

Identyfikatory

DOI

10.24425/amm.2020.133705

• Języki publikacji: EN

Abstrakty

EN

In the present study, the lead-free BaTi_1-x Zr_x O₃ (for x = 0, 0.05 and 0.15) ceramics were prepared by High-Energy Ball Milling and heat treatments. The performed X-ray, SEM and EDS measurements confirmed high purity, good quality and the expected quantitative composition of the obtained samples. The study of dielectric properties was performed by means of broadband dielectric spectroscopy at the frequency ranging from 0.1 Hz to 10 MHz. The obtained measurement data, analyzed in accordance with the Arrhenius formalism demonstrated the presence of relaxation type dielectric mechanisms. The impedance answer of studied ceramic materials indicated the presence of two relaxation processes: one with a dominant resistive component and the other with a small capacitive component. The observed dielectric relaxation process is temperature dependent and has a “non-Debye” character.

Słowa kluczowe

EN

BaTiO3; mechanochemical synthesis; X-ray methods; dielectric properties

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2020
• Tom: Vol. 65, iss. 4
• Strony: 1391--1396
• Opis fizyczny: Bibliogr. 31 poz., fot., rys.

Twórcy

autor

Garbarz-Glos B.

• Institute of Technology, Pedagogical University of Cracow, 2 Podchorążych Str., 30-084 Kraków, Poland

autor

Bąk W.

• Institute of Technology, Pedagogical University of Cracow, 2 Podchorążych Str., 30-084 Kraków, Poland

autor

Budziak A.

• AGH University of Science and Technology, Faculty of Energy and Fuels, Al. Mickiewicza 30, 30-059 Kraków, Poland

autor

Dulian P.

• Cracow University of Technology, Faculty of Chemical Engineering and Technology, 24 Warszawska Str., 31-155 Kraków, Poland

autor

Lisińska-Czekaj A.

• Gdańsk University of Technology, Faculty of Mechanical Engineering, Department of Materials Engineering and Welding, 11/12 G. Narutowicza Str., 80-233, Gdańsk, Poland

autor

Czekaj D.

• Gdańsk University of Technology, Faculty of Mechanical Engineering, Department of Materials Engineering and Welding, 11/12 G. Narutowicza Str., 80-233, Gdańsk, Poland

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