Fabrication and characterization of Zr microplasma sprayed coatings for medical applications

• Autorzy: Voinarovych Sergii G. , Alontseva Darya L. , Kyslytsia Oleksandr N. , Kaliuzhnyi Sergii , Khozhanov Alexandr R. , Krasavin Alexander , Kolesnikova Tatiana

Identyfikatory

DOI

10.2478/adms-2021-0013

• Języki publikacji: EN

Abstrakty

EN

This paper presents new results of studying the influence of parameters of microplasma spraying (MPS) of Zr wire on the structure of Zr coatings. The coating experiments were accomplished in a two level fractional factorial design. Individual particles of sprayed Zr wire and their splats on the substrate were collected under various spraying parameters (amperage, spraying distance, plasma gas flow rate and wire flow rate) and evaluated by Scanning Electron Microscopy (SEM) to establish the effect of particle size and shape on the coating microstructure. The particles were characterized by measurement of their sizes and the obtained results were evaluated in terms of their degree of melting. This was compared with the experimentally observed coating microstructure type and finally correlated to the investigated coating porosity to select the specific MPS parameters of Zr coatings depositing onto medical implants from Ti alloy. It was found that the main parameters influencing the size of the sprayed Zr particles and the porosity of the Zr coatings are the plasma gas flow rate and amperage. It was demonstrated that it is possible to control the porosity of Zr microplasma coatings in the range from 2.8% to 20.3% by changing the parameters of the MPS. The parameters of microplasma spraying of Zr wire were established to obtain medical implant coatings with porosity up to 20.3% and pore size up to 300 μm.

Słowa kluczowe

EN

zirconium coatings; titanium implants; microplasma spraying; MPS; porosity; splats; scanning electron microscopy; SEM

PL

powłoka cyrkonowa; implanty tytanowe; natryskiwanie mikroplazmowe; porowatość; skaningowa mikroskopia elektronowa

• Wydawca: Politechnika Gdańska
• Czasopismo: Advances in Materials Science
• Rocznik: 2021
• Tom: Vol. 21, nr 2(68)
• Strony: 93--105
• Opis fizyczny: Bibliogr. 35 poz., tab., wykr., il.

Twórcy

autor

Voinarovych Sergii G.

• E.O. Paton Electric Welding Institute, Ukraine

autor

Alontseva Darya L.

• D. Serikbayev East Kazakhstan Technical University, Ust-Kamenogorsk, Kazakhstan

autor

Kyslytsia Oleksandr N.

• E.O. Paton Electric Welding Institute, Ukraine

autor

Kaliuzhnyi Sergii

• E.O. Paton Electric Welding Institute, Ukraine

autor

Khozhanov Alexandr R.

• D. Serikbayev East Kazakhstan Technical University, Ust-Kamenogorsk, Kazakhstan

autor

Krasavin Alexander

• D. Serikbayev East Kazakhstan Technical University, Ust-Kamenogorsk, Kazakhstan

autor

Kolesnikova Tatiana

• D. Serikbayev East Kazakhstan Technical University, Ust-Kamenogorsk, Kazakhstan

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Uwagi

1. Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).

2. The work was supported by the National Academy of Science of Ukraine under Grant number 0117U004951