Physical aging of polylactide-valsartan system investigated by differential scanning calorimetry

• Autorzy: Drogoń Agata , Skotnicki Marcin , Pyda Marek

Identyfikatory

DOI

10.14314/polimery.2020.7.5

Warianty tytułu

PL

Proces fizycznego starzenia układów polilaktyd-walsartan badany metodą różnicowej kalorymetrii skaningowej

• Języki publikacji: EN

Abstrakty

EN

The polylactide-valsartan systems with a mass ratio of 20 : 80, 50 : 50 and 80 : 20 were obtained and characterized by standard Differential Scanning Calorimetry (DSC). The isothermal physical aging process of polylactide-valsartan with a mass ratio of 50 : 50 was investigated at the aging temperature of 50°C and 70°C for different aging times. The enthalpy of relaxation values for each of the aging times and for all investigated components were determined experimentally and fitted to the Kohlrausch-Williams-Watts equation.

PL

Otrzymane układy polilaktydu z walsartanem w stosunkach masowych 20 : 80, 50 : 50 i 80 : 20 poddano analizie metodą różnicowej kalorymetrii skaningowej (DSC). Scharakteryzowano proces starzenia fizycznego mieszaniny polilaktyd-walsartan w stosunku masowym 50 : 50, prowadzony w temperaturze 50 i 70°C w różnym czasie. Z pomiarów doświadczalnych dla każdego czasu starzenia wyznaczono entalpię relaksacji, a następnie dopasowano otrzymane wielkości do równania Kohlrauscha-Williamsa-Wattsa.

Słowa kluczowe

EN

physical aging; enthalpy relaxation; polylactide; valsartan; Differential Scanning Calorimetry (DSC); Kohlrausch-Williams-Watts equation (KWW)

PL

starzenie fizyczne; entalpia relaksacji; polilaktyd; walsartan; różnicowa kalorymetria skaningowa (DSC); równanie Kohlrauscha-Williamsa-Wattsa (KWW)

• Wydawca: Sieć Badawcza Łukasiewicz – Instytut Chemii Przemysłowej
• Czasopismo: Polimery
• Rocznik: 2020
• Tom: T. 65, nr 7-8
• Strony: 533--541
• Opis fizyczny: Bibliogr. 55 poz., rys. kolor.

Twórcy

autor

Drogoń Agata

• Rzeszów University of Technology, Department of Chemistry, al. Powstańców Warszawy 6, 35-959 Rzeszów, Poland

autor

Skotnicki Marcin

• Poznań University of Medical Sciences, Department of Pharmaceutical Technology, Grunwaldzka 6, 60-780 Poznań, Poland

autor

Pyda Marek

• Rzeszów University of Technology, Department of Chemistry, al. Powstańców Warszawy 6, 35-959 Rzeszów, Poland
• Poznań University of Medical Sciences, Department of Biophysics, Grunwaldzka 6, 60-780 Poznań, Poland

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Uwagi

PL

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).