Characterization of a static expansion standard for calibrating medium and high vacuum pressure gauges

• Autorzy: Duarte Franco Jonathan Javier , Villamizar Mora Carlos Mauricio , García Sánchez Carlos Eduardo

Identyfikatory

DOI

10.24425/mms.2021.137137

• Języki publikacji: EN

Abstrakty

EN

The Centro de Desarrollo Tecnológico del Gas developed a static expansion system to enable the calibration of medium and high vacuum pressure gauges in Colombia. The system can generate pressures between 0.1 Pa and 100 kPa. The characterization tests included the evaluation of pressure stability and desorption rate, a trueness test, and the analysis of the uncertainty budget of the calibration result. The pressure stability test was successfully completed and showed the positive effect of baking on the final pressure in the system. The trueness test allowed concluding that the calibration results with the system are comparable with those obtained with a reference meter traceable to a national metrology institute. The uncertainty budget analysis indicated the dominance of the pressure of the unit under calibration and of the initial pressure in the small tank in different pressure ranges on the uncertainty of the result. A comparison with a Monte Carlo simulation led to the conclusion that in this situation, the GUM (Guide to the Expression of Uncertainty in Measurement) method is not ideal for estimating the uncertainty of the results.

Słowa kluczowe

EN

static expansion system; calibration; vacuum; characterization

• Wydawca: Komitet Metrologii i Aparatury Naukowej PAN
• Czasopismo: Metrology and Measurement Systems
• Rocznik: 2021
• Tom: Vol. 28, nr 3
• Strony: 593--604
• Opis fizyczny: Bibliogr. 19 poz., rys., tab., wykr., wzory

Twórcy

autor

Duarte Franco Jonathan Javier

• Corporación Centro de Desarrollo Tecnológico del Gas, Grupo de Investigación en Fluidos y Energía, Carrera 23 # 106-08, ZIP 680004, Bucaramanga, Colombia

autor

Villamizar Mora Carlos Mauricio

• Universidad Industrial de Santander, Escuela de Ingeniería Mecánica, Grupo de Investigación en Energía y Medio Ambiente, Carrera 27 calle 9, ZIP 680002, Bucaramanga, Colombia

autor

García Sánchez Carlos Eduardo

• Corporación Centro de Desarrollo Tecnológico del Gas, Grupo de Investigación en Fluidos y Energía, Carrera 23 # 106-08, ZIP 680004, Bucaramanga, Colombia

Bibliografia

• [1] Khan, W., Hong, H. H., Satar, T., Ahmed, M., Khan, Z. A., & Khan, M. Z. (2016). The KRISS primary vacuum gauge calibration standards: A review. Journal of the Vacuum Society of Japan, 59(8), 222-235.
• [2] Astrua, M., Mari, D., & Pasqualin, S. (2019). Improvement of INRiM static expansion system as vacuum primary standard between 10-4 Pa and 1000 Pa. 19th International Congress of Metrology, 27007. https://doi.org/10.1051/metrology/201927007
• [3] Semwal, P., Khan, Z., Dhanani, K. R., Pathan, F. S., George, S., Raval, D. C., Thankey, P. L., Paravastu, Y., & Himabindu, M. (2012). Spinning rotor gauge based vacuum gauge calibration system at the Institute for Plasma Research. Journal of Physics: Conference Series, 390, 012027. https://doi.org/10.1088/1742-6596/390/1/012027
• [4] Bergoglio, M., & Calcatelli, A. (2004). Uncertainty evaluation of the IMGC-CNR static expansion system. Metrologia, 41, 278-284. https://doi.org/10.1088/0026-1394/41/4/009
• [5] Greenwood, J. C. (2006). Simulation of the operation and characteristics of static expansion pressure standards. Vacuum, 80, 548-553. https://doi.org/10.1016/j.vacuum.2005.09.003
• [6] Soriano Cardona, B., Torres Guzmán, J., & Santander Romero, L. (2001). Sistema de referencia nacional para la medición de vacío. Simposio de Metrología CENAM 2001, México.
• [7] Bergoglio, M., Calcatelli, A., Marzola, L., & Rumiano, G. (1988). Primary pressure measurements down to 10-6 Pa. Vacuum, 38(8-10), 887-891. https://doi.org/10.1016/0042-207X(88)90486-1
• [8] Fedchak, J. A., Abbott, P. J., & Hendricks, J. H. (2018). Review Article: Recommended practice for calibrating vacuum gauges of the ionization type. Journal of Vacuum Science & Technology A, 36, 030802. https://doi.org/10.1116/1.5025060
• [9] Torres Guzmán, J. C., Santander, L. A., & Jousten, K. (2005). Realization of the medium and high vacuum primary standard in CENAM, Mexico. Metrologia, 42(6), S157-S160. https://doi.org/10.1088/0026-1394/42/6/S01
• [10] Jousten, K., Röhl, P., & Aranda Contreras, V. (1999). Volume ratio determination in static expansion systems by means of a spinning rotor gauge. Vacuum, 52(4), 491-499. https://doi.org/10.1016/S0042-207X(98)00337-6
• [11] Herranz, D., Ruiz, S., & Medina, N. (2009). Volume ratio determination in static expansion systems by means of two pressure balances. XIX IMEKO World Congress, Fundamental and Applied Metrology, Portugal. https://www.imeko2009.it.pt/Papers/FP_280.pdf
• [12] Phanakulwijit, S., & Pitakarnnop, J. (2019). Establishment of Thailand’s national primary vacuum standard by a static expansion method. Journal of Physics: Conference Series, 1380, 012003. https://doi.org/10.1088/1742-6596/1380/1/012003
• [13] Jitschin, W. (2002). High-accuracy calibration in the vacuum range 0.3 Pa to 4000 Pa using the primary standard of static gas expansion. Metrologia, 39(3), 249-261. https://doi.org/10.1088/0026-1394/39/3/2
• [14] Kangi, R., Ongun, B., & Elkatmis, A. (2004). The new UME primary standard for pressure generation in the range from 9 ×10-4 Pa to 103 Pa. Metrologia, 41(4), 251-256. https://doi.org/10.1088/0026-1394/41/4/005
• [15] International Organization for Standardization. (2011). Vacuum gauges - Calibration by direct comparison with a reference gauge ISO Standard No. 3567:2011. https://www.iso.org/standard/59372.html
• [16] Antsukova, A. I., Gorobei, V. N., Liubomirov, A. B., Pimenova, A. A., & Chernyshenko, A. A. (2019). Calibration of measuring instruments of low absolute pressures. IOP Conference Series: Journal of Physics: Conference Series, 1313, 012002. https://doi.org/10.1088/1742-6596/1313/1/012002
• [17] Ruiz González, S. (2011). Desarrollo de un nuevo patrón nacional de presión. Desde la columna de mercurio a patrones primarios de vacío [Doctoral dissertation, Universidad de Valladolid]. UVaDOC Repositorio Documental de la Universidad de Valladolid. https://doi.org/10.35376/10324/830
• [18] Joint Committee for Guides in Metrology. (2008). Evaluation of measurement data - Guide to the expression of uncertainty in measurement (JCGM 100:2008). http://www.bipm.org/utils/common/documents/jcgm/JCGM_100_2008_E.pdf
• [19] Joint Committee for Guides in Metrology. (2008). Evaluation of measurement data - Supplement 1 to the “Guide to the expression of uncertainty in measurement” - Propagation of distributions using a Monte Carlo method (JCGM 101:2008). https://www.bipm.org/documents/20126/2071204/JCGM_101_2008_E.pdf

Uwagi

1. This work was financed by Colombia’s Servicio Nacional de Aprendizaje (SENA) through the Special Cooperation Agreement no. 0233 of 2018. SENA’s Centro Industrial del Diseño y la Manufactura and Centro Industrial y del Desarrollo Tecnológico participated in the project transfer plan.

2. Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).