Synthesis of conical Co–Fe alloys structures obtained with crystal modifier in superimposed magnetic field

• Autorzy: Skibińska Katarzyna , Kutyła Dawid , Kołczyk-Siedlecka Karolina , Marzec Mateusz M. , Żabiński Piotr , Kowalik Remigiusz

Identyfikatory

DOI

10.1007/s43452-021-00315-2

• Języki publikacji: EN

Abstrakty

EN

The addition of crystal modifier to electrolyte used during electrodeposition of metals and alloys allows obtaining conical structures without using any template. This method is fast and ensures covering large areas during one single electrodeposition process. In this work, Co–Fe cones were obtained by one-step method with ammonium chloride as a crystal modifier. The influence of electrodeposition parameters and electrolyte compositions were investigated. Electrodeposition conditions (duration, electrolyte temperature, and addition of NH4Cl), which allow obtaining the most uniform conical structures, were applied during sample fabrication in the magnetic field. The influence of its value and direction on the quality and compositions of obtained alloys was investigated using Scanning Electron Microscope (SEM) photos. To check if there is any change in the sample crystal system, the X-Ray Diffraction (XRD) analysis was performed. To confirm the synthesis of Co–Fe cones, they were analyzed using the X-ray photoelectron Spectroscopy (XPS) method.

Słowa kluczowe

EN

Co-Fe alloy; crystal modifier; conical structures; magnetic field; free-standing structures

PL

stop Co-Fe; pole magnetyczne; konstrukcja wolnostojąca

• Wydawca: Springer ; Wrocław University of Science and Technology
• Czasopismo: Archives of Civil and Mechanical Engineering
• Rocznik: 2021
• Tom: Vol. 21, no. 4
• Strony: 507--517
• Opis fizyczny: Bibliogr. 28 poz., rys., wykr.

Twórcy

autor

Skibińska Katarzyna

• Faculty of Non-Ferrous Metals, AGH University of Science and Technology, A. Mickiewicza 30, 30-059 Krakow, Poland

• https://orcid.org/0000-0002-0332-7725

autor

Kutyła Dawid

• Faculty of Non-Ferrous Metals, AGH University of Science and Technology, A. Mickiewicza 30, 30-059 Krakow, Poland

• https://orcid.org/0000-0002-6482-0740

autor

Kołczyk-Siedlecka Karolina

• Faculty of Non-Ferrous Metals, AGH University of Science and Technology, A. Mickiewicza 30, 30-059 Krakow, Poland

• https://orcid.org/0000-0002-8391-4603

autor

Marzec Mateusz M.

• Academic Centre for Materials and Nanotechnology, AGH University of Science and Technology, A. Mickiewicza 30, 30-059 Krakow, Poland

• https://orcid.org/0000-0001-9834-3930

autor

Żabiński Piotr

• Faculty of Non-Ferrous Metals, AGH University of Science and Technology, A. Mickiewicza 30, 30-059 Krakow, Poland

• https://orcid.org/0000-0002-5085-2645

autor

Kowalik Remigiusz

• Faculty of Non-Ferrous Metals, AGH University of Science and Technology, A. Mickiewicza 30, 30-059 Krakow, Poland

• https://orcid.org/0000-0002-3942-2521

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Uwagi

PL

Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023)