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Properties of Ti-6Al-7Nb titanium alloy nitrocarburized under glow discharge conditions

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The paper presents the results of physicochemical and mechanical properties of the Ti-6Al-7Nb alloy with surface modified by formation of a diffusive nitrocarburized layer deposited in a low-temperature plasma process. The main aim of the study was to evaluate the influence of steam sterilization and exposure to Ringer’s solution on the utility properties of the alloy. Methods: Based on the study of the microstructure, roughness, wettability, resistance to pitting corrosion, ion infiltration and mechanical properties, the usefulness of the proposed method of surface treatment for clinical application was proven. Results: Deposition of the nitrocarburized layer increased the surface roughness and surface hardness, but also reduced the contact angle, and corrosion resistance with respect to the polished surfaces. The nitrocarburized layer is a barrier against the infiltration of ions to the solution and sterilization and exposure to Ringer solution have greater effect on the physicochemical properties rather than on the mechanical ones. Conclusion: It was found that sterilization, and exposure to Ringer’s solution greatly affect the change of physicochemical properties rather than mechanical properties for both nitrocarburized layers and the Ti-6Al-7Nb alloy of mechanically polished surface.
Rocznik
Strony
181--188
Opis fizyczny
Bibliogr. 27 poz., rys., tab., wykr.
Twórcy
autor
  • Faculty of Biomedical Engineering, Silesian University of Technology, Zabrze, Poland
  • Faculty of Biomedical Engineering, Silesian University of Technology, Zabrze, Poland
autor
  • Faculty of Biomedical Engineering, Silesian University of Technology, Zabrze, Poland
autor
  • Faculty of Mining and Geology, Silesian University of Technology, Gliwice, Poland
autor
  • Faculty of Biomedical Engineering, Silesian University of Technology, Zabrze, Poland
autor
  • Warsaw University of Technology, Faculty of Materials Science and Engineering, Warsaw, Poland
  • Warsaw University of Technology, Faculty of Materials Science and Engineering, Warsaw, Poland
Bibliografia
  • [1] BASIAGA M., KAJZER W., WALKE W., KAJZER A., KACZMAREK M., Evaluation of physicochemical properties of surface modified Ti6Al4V and Ti6Al7Nb alloys used for orthopeadic implants, Mat. Sci. Eng. C-Mater., 2016, 68, 851–860.
  • [2] BASIAGA M., WALKE W., PASZENDA Z., KAJZER A., The effect of EO and steam sterilization on mechanical and electrochemical properties of titanium grade 4, Mater. Technol., 2016, 50(1), 153–158.
  • [3] BRUNETTE D.M., TENGVALL P., TEXTOR M., THOMSEN P., Titanium in Medicine, Springer-Verlag, Berlin, Heidelberg, 2001.
  • [4] CHRZANOWSKI W., Corrosion behavior of Ti-6Al-7Nb alloy after different surface treatments, JAMME, 2006, 18, 67–70.
  • [5] CZARNOWSKA E., MORGIEL J., OSSOWSKI M., MAJOR R., WIERZCHOŃ T., Microstructure and biocompatibility of titanium oxide produced on nitrided surface layer under glow discharge conditions, J. Nanosci. Nanotechnol., 2011, 11(10), 8917–8923.
  • [6] CZARNOWSKA E., WIERZCHOŃ T., MARANDA A., KACZMAREWICZ E., Improvement of titanium alloy for biomedical applications by nitriding and carbonitriding process under glow discharge conditions, J. Mater. Sci.: Med. Mat., 2000, 11(2), 73–81.
  • [7] FARÈ S., LECIS N., VEDANI M., SILIPIGNI A., FAVOINO P., Properties of nitrided layers formed during plasma nitriding of commercially pure Ti and Ti-6Vl-4V alloy, Surf. Coat. Tech., 2012, 206, 2287–2292.
  • [8] FAROKHZADEH K., EDRISY A., PIGOTT G., LIDSTER P., Scratch resistance analysis of plasma-nitrided Ti-6Al-4V alloy, Wear, 2013, 302, 845–853.
  • [9] FLESZAR A., WIERZCHOŃ T., SUN K.K., SOBIECKI J.R., Properties of surface layers produced on the Ti6Al2Cr2Mo titanium alloy inder glow discharge conditions, Surf. Coat. Tech., 2001, 31, 73–81.
  • [10] GEETHA M., SING A.K., ASOKAMANI R., GOGIA A.K., Ti based biomaterials, the ultimate choice for othopaedic implants – a review, Prog. Mater. Sci., 2009, 54, 397–425.
  • [11] GOKUL LAKSHMI S., RAMAN V., RAJENDRAN N., BABI M.A.K., ARIVUOLI D., In vitro behavior of plasma nitrided Ti-6Al-7Nb orthopaedic alloy in Hanks solution, Sci. Technol. Adv. Mat., 2003, 4, 415–418.
  • [12] KIEL M., SZEWCZENKO J., BASIAGA M., NOWIŃSKA K., Technological capabilities of surface layers formation on implants made of Ti-6Al-4V alloy, Acta Bioeng. Biomech., 2015, 17(1), 31–37.
  • [13] LUKINA E., LAKA A., KOLLEROV M., SAMPIEV M., MASON P., WAGSTAFF P., NOORDEEN H., YOON W.W., BLUNN G., Metal concectrations in the blood and tissues after implantation of titanium growth guidance sliding instrumentation, Spine J., 2016, 16(3), 380–388.
  • [14] MARCINIAK J., SZEWCZENKO J., KAJZER W., Surface modification of implants for bone surgery, Arch. Metal. Mater., 2015, 60(3B), 2123–2129.
  • [15] MARCINIAK J., Biomateriały, Wydawnictwo Politechniki Śląskiej, Gliwice, 2013, (in Polish).
  • [16] MARCINIAK J., CHRZANOWSKI W., KAJZER A., Gwoździowanie śródszpikowe w osteosyntezie, Wydawnictwo Politechniki Śląskiej, Giwice, 2008, (in Polish).
  • [17] OKAZAKI Y., GOTOH E., Comparison of metal release from various metallic biomaterials in vitro, Biomaterials, 2005, 26, 11–20.
  • [18] OKAZAKI Y., ITO Y., New Ti alloy without Al and V for medical implants, Adv. Eng. Mater., 2000, 2(5), 278–281.
  • [19] RAHMAN M., REID I., DUGGAN P., DOWLING D.P., HUGHES G., HASHMI M.S.J., Structural and tribological properties of the plasma nitrided Ti-alloy biomaterials: Influence of the treatment temperature, Surf. Coat. Tech., 2007, 201, 4865–4872.
  • [20] SEMLISCH M., STAUB F., WEBER H., Develompent of vital highstrength Ti-Al-Nb alloy for surgical implants, [in:] P. Christer, A. Meunier, A.J.C. Lee (eds.), Perfomance of Biomaterials, Elsevier Science Publishers, Amsterdam, 1986, 69–74.
  • [21] THAIR L., KAMACHI MUDALI U., BHUVANESWARAN N., NAIR K.G.M., ASOKAMANI R., RAJ B., Nitrogen ion implantation and in vitro behavior of as-cast Ti-6Al-7Nb alloy, Corros. Sci., 2002, 44(11), 2439–2457.
  • [22] THIERRY B., TABRIZIAN M., SAVADOGO O., YAHIA L., Effects of sterilization processes on NiTi alloy, surface characterization, J. Biomed. Mater. Res., 2000, 49(1), 88–98.
  • [23] WALKE W., BASIAGA M., PASZENDA Z., MARCINIAK J., Physicochemical properties of Ti67 alloy after EO and stem sterilization, Mater. Technol., 2016, 50(3), 323–329.
  • [24] WALKE W., PASZENDA Z., KARASIŃSKI P., MARCINIAK J., BASIAGA M., Investigations of mechanical properties of SiO2/TiO2 coatings deposited by sol-gel method on cpTi and Ti-6Al-7Nb, Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications, 2016, 230, 3, 799–804
  • [25] WIERZCHOŃ T., CZARNOWSKA E., GRZONKA J., SOWIŃSKA A., TARNOWSKI M., KAMIŃSKI J., BOROWSKI T., KURZYDŁOWSKI K.J., Glow discharge assisted oxynitriding process of tinanium for medical application, Appl. Surf. Sci., 2015, 334, 74–79
  • [26] WIERZCHOŃ T., SOBIECKI J.R., KRUPA D., The formation of Ti(OCN) layers produced from metal-organic compounds using plasma assisted chemical vapor deposition, Surf. Coat. Tech., 1993, 59(1–3), 217–220.
  • [27] WIERZCHOŃ T., CZARNOWSKA E., MORGIEL J., SOWIŃSKA A., TARNOWSKI M., ROGUSKA A., The importance of surface topography for the biological properties of nitrided diffusion layer produced on Ti6Al4V titanium alloy, Arch. Metalland. Mater., 2015, 60, 2153–2159.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-d7d13dca-ac1b-404d-9fd9-1a5950c60491
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