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Transmission electron microscope studies on carbon nanostructured materials

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Wybrane pełne teksty z tego czasopisma
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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: Carbon nanostructured materials are important and still not satisfactorily recognised products. Structure can be investigated with sufficient resolution using transmission electron microscopy but main difficulties are connected with low scattering of electrons by carbon atoms and destruction by knock-on damage caused by collisions of high energy electrons with specimen atoms. Design/methodology/approach: Scanning/transmission electron microscopy (S/TEM) deliver a chance to improve the quality of performed investigations. BF, DF and HAADF detectors were applied for various carbon materials: carbon nanotubes, nano-onions, nanodiamonds and graphitized carbon black. Findings: Obtained results confirmed the usefulness of applied microscopy techniques. Research limitations/implications: Sample preparation is crucial for performed investigations. Because of ionization damage caused by collisions of high energy electrons, results obtained with high-voltage TEM have to be analysed with caution, hence low-voltage electron microscopy is strongly recommended. Originality/value: New and not commonly used techniques were applied for carbon nanostructured materials studies. Advantages and disadvantages of them were compared.
Rocznik
Strony
58--67
Opis fizyczny
Bibliogr. 17 poz.
Twórcy
autor
  • Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
Bibliografia
  • [1]J.L. Delgado, M.A. Herranz, N. Marti, The nano-forms of carbon, Journal of Materials Chemistry 18 (2008) 1417-1426.
  • [2]L.A. Dobrzański, M. Pawlyta, A. Hudecki, Conceptual study on a new generation of the high-innovative advanced porous and composite nanostructural functional materials with nanofibers, Journal of Achievements in Materials and Manufacturing Engineering 49/2 (2011) 550-565.
  • [3]K. Mitura, HR TEM examinations of nanodiamond particles for biomedical application, Journal of Achievements in Materials and Manufacturing Engineering 37/2 (2009) 317-320
  • [4]L.A. Dobrzański, M. Pawlyta, A. Krztoń, B. Liszka, K. Labisz, Synthesis and characterization of carbon nanotubes decorated with platinum nanoparticles, Journal of Achievements in Materials and Manufacturing Engineering 39/2 (2010) 184-189.
  • [5]R.E. Franklin, The interpretation of diffuse X-ray diagrams of carbon, Acta Crystallographica 3 (1950) 107-121.
  • [6]R.E. Franklin, Crystallite growth in graphitizing and non-graphitizing carbons, Proceedings of the Royal Society A 209 (1951) 196-218.
  • [7]A. Oberlin, Application of dark-field electron microscopy to carbon study, Carbon 17/1 (1979) 7-20.
  • [8]A. Oberlin, Carbonization and graphitization, Carbon 22/6 (1984) 521-541.
  • [9]D.C. Bell, N. Erdman, Low voltage electron microscopy, principles and applications (RMS - Royal Microscopical Society), John Wiley and Sons, 2013.
  • [10]J.R. Jinschek, E. Yucelen, H.A. Calderon, B. Freitag, Quantitative atomic 3-D imaging of single/double sheetgraphene structure, Carbon (2011) 556-562.
  • [11]J.N. Rouzaud, C. Clinard, Quantitative high-resolution transmission electron microscopy, a promising tool for carbon materials characterization, Fuel Processing Technology 77-78 (2002) 229-235.
  • [12]Z. Kaszkur, J. Pilaszek, E. Trzetrzewinska, Analysis of highangle diffraction patterns obtained for solid carbon materials, XRD diffraction method for carbon structure investigation, Publishing House of Wojciech Swietosławski Foundation, Gliwice, 1993, 59-75 (in Polish).
  • [13] P.J.F. Harris, A. Burian, S. Duber, High-resolution electron microscopy of a microporous carbon, Philosophical Magazine Letters 80/6 (2000) 381-386.
  • [14] R. Brydson, Aberration-corrected Analytical Electron Microscopy (RMS - Royal Microscopical Society), John Wiley and Sons, 2011
  • [15] C.L. Guillou, F. Brunet, T. Irifune, H. Ohfuji, J.N. Rouzaud, Nanodiamond nucleation below 2273 K at 15 GPa from carbons with different structural organizations, Carbon 45/3 (2007) 636-648.
  • [16] W.M. Hess, C.R. Herd, Microstructure, morphology and general physical properties, Carbon Black, Dekker, New York, 1993, 89-173.
  • [17] R.D. Heidenreich, W.M. Hess, L.L. Ban, Structure of spherule and layers inferred from electron microscopy and X-ray diffraction, Journal of Applied Crystallography 1 (1968) 1-19.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-d68903bd-4bf6-4e16-b22f-ed5958d73b51
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