Determination of silodosin in biological samples using UPLC–MS/MS combined with magnetic carboxylated multiwalled carbon nanotubes

• Autorzy: Yin Q. H. , Zhu Y. Q. , Yang Y. L.

Identyfikatory

DOI

10.1556/1326.2016.00150

• Języki publikacji: EN

Abstrakty

EN

Novel magnetic solid-phase extraction using carboxylated multiwalled carbon nanotubes was proposed with ultra high-performance liquid chromatography–tandem mass spectrometry for the determination of silodosin in biological samples. The effects of various experimental parameters including adsorbent amount, pH, adsorption time, desorption conditions, and adsorbent reusability were systematically validated. Under the optimized conditions, the calibration curve was linear within the concentration range of 1.0–800 ng mL−1 with the correlation coefficient of 0.9997 and the lower limit of detection was 0.3 ng mL−1. The extraction recoveries were over 90.0% with relative standard deviation (RSD) of less than 5.0%. All these results suggested that magnetic extraction method can be used for enrichment and quantification of silodosin in biological samples.

Słowa kluczowe

EN

Silodosin; magnetic solid-phase extraction; multiwalled carbon nanotubes; biological samples; UPLC–MS/MS

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2018
• Tom: Vol. 30, no. 1
• Strony: 47--53
• Opis fizyczny: Bibliogr. 36 poz., rys.

Twórcy

autor

Yin Q. H.

• Faculty of Environmental Science and Engineering, Kunming University of Science and Technology, Kunming 650500, Yunnan, China
• Faculty of Life Science and Technology, Kunming University of Science and Technology, Kunming 650500, Yunnan, China
• Kunming Jida Pharmaceutical Co., Ltd., Kunming 650106, Yunnan, China

autor

Zhu Y. Q.

• Faculty of Environmental Science and Engineering, Kunming University of Science and Technology, Kunming 650500, Yunnan, China
• Research Center for Analysis and Measurement, Kunming University of Science and Technology, Kunming 650093, China
• Faculty of Life Science and Technology, Kunming University of Science and Technology, Kunming 650500, Yunnan, China

autor

Yang Y. L.

• Faculty of Life Science and Technology, Kunming University of Science and Technology, Kunming 650500, Yunnan, China

Bibliografia

• [1] Oesterling, J. E. New Engl. J. Med. 1995 , 332 , 99 – 109.
• [2] Yoshida, M. ; Homma, Y. ; Kawabe K. Expert. Opin. Inv. Drug. 2007 , 16 , 1955 – 1965 .
• [3] Masaji, I. ; Yukiyo, F. ; Toshio, O. ; Maruf, A. ; Ikunobu, M. ; Takafumi N. Life Sci. 2002 , 71 , 2531 – 2541 .
• [4] Murata, S. ; Taniguchi, T. ; Takahashi, M. ; Okada, K. ; Akiyama, K. ; Muramatsu I. J. Urology 2000 , 164 , 578 – 583 .
• [5] Kawabe, K. ; Yoshida M. ; Homma, Y. Brit. J. Urol. Int. 2006 , 98 , 1019 – 1024 .
• [6] Jahan, K. K. ; Malipatil, S. M. Int. J. Pharm. Res. Anal. 2014 , 4 , 65 – 69 .
• [7] Jahan, K. K. ; Malipatil, S. M. World J. Pharm. Pharm. Sci. 2014 , 3 , 960 – 969 .
• [8] Aneesh, T. P. ; Rajasekaran, A. Int. J. Biol. Pharm. Res. 2012 , 3 , 693 – 696 .
• [9] Shaik, J. V. ; Saladi, S. ; Sait, S. S. J. Chromatogr. Sci. 2014 , 52 , 646 – 653 .
• [10] Zhao, X. ; Liu, Y. W. ; Xu, J. Y. ; Zhang, D. ; Zhou, Y. ; Gu, J. K. ; Cui, Y. M. J. Chromatogr. B. 2009 , 877 , 3724 – 3728 .
• [11] Er, E. ; Çelikkan, H. ; Erk, N. ; Aksu, M. L. Electrochim. Acta 2015 , 157 , 252 – 257 .
• [12] Lijima, S. Nature 1991 , 354 , 56 – 58 .
• [13] Latorre, C. H. ; Mendez, J. A. ; Garcia, J. B. ; Martin, S. G. ; Crecente, R. M. P. Anal. Chim. Acta 2012 , 749 , 16 – 35 .
• [14] Su, S. W. ; Liao, Y. C. ; Whang, C. W. J. Sep. Sci. 2012 , 35 , 681 – 687 .
• [15] Yin, Q. H. ; Zhu, Y. Q. ; Ju, S. Q. ; Liao, W. L. ; Yang, Y. L. Res. Chem. Intermediat. 2016 , 42 , 4985 – 4998 .
• [16] Chatterjee, J. ; Haik, Y. ; Chen, C. J. J. Magn. Magn. Mater. 2001 , 225 , 21 – 29 .
• [17] Jordan, A. ; Scholz, R. ; Wust, P. ; Fahling, H. ; Felix, R. J. Magn. Magn. Mater. 1999 , 201 , 413 – 419 .
• [18] Abdolmohammad-Zadeh, H. ; Talleb, Z. Talanta 2015 , 134 , 387 – 393 .
• [19] Liu, J. F. ; Yuan, B. F. ; Feng, Y. Q. Talanta 2015 , 136 , 54 – 59 .
• [20] Asgharinezhad, A. A. ; Ebrahimzadeh, H. ; Mirbabaei, F. ; Mollazadeh, N. ; Shekari, N. Anal. Chim. Acta 2014 , 844 , 80 – 89 .
• [21] Rezazadeh, M. ; Yamini, Y. ; Seidi, S. J. Chromatogr. A 2015 , 1396 , 1 – 6 .
• [22] Xiao, D. L. ; Zhang, C. ; Yuan, D. H. ; He, J. ; Wu, J. R. ; Zhang, K. ; Lin, R. ; He, H. RSC Adv. 2014 , 110 , 64843 – 64854 .
• [23] Huang, H. ; Liu, X. M. ; Zhang, X. Y. ; Liu, W. L. ; Su, X. G. ; Zhang, Z. Q. Electroanal. 2010 , 22 , 433 – 438 .
• [24] Baby, T. T. ; Ramaprabhu, S. Talanta 2010 , 80 , 2016 – 2022 .
• [25] Song, H. J. ; Li, N. ; Jing, X. J. ; Yang, X. F. ; Tang, H. J. Nanopart. Res. 2011 , 13 , 5457 – 5464 .
• [26] Pawar, S. P. ; Gandi, M. ; Bose, S. RSC Adv. 2016 , 6 , 37633 – 37645 .
• [27] Tao, Y. ; Jiang, Y. H. ; Li, W. D. ; Cai, B. C. RSC Adv. 2016 , 6 , 34782 – 34790 .
• [28] Maher, H. M. ; Alzoman, N. Z. ; Alshehri, M. M. ; Aljohar, H. I. ; Shehata, S. ; Alossaimi, M. ; Abanmy, N. O. RSC Adv. 2015 , 5 , 98600 – 98609 .
• [29] Xiao, D. L. ; Dramou, P. ; Xiong, N. Q. ; Hua, H. ; Li, H. ; Yuan, D. H. ; Dai, H. J. Chromatogr. A 2013 , 1274 , 44 – 53 .
• [30] Baykal, A. ; Senel, M. ; Unal, B. ; Karaoglu, E. ; Sozeri, H. ; Toprak, M. S. J. Inorg. Organomet. P. 2013 , 23 , 726 – 735 .
• [31] Yuen, S. M. ; Ma, C. C. M. ; Chiang, C. L. Compos. Sci. Technol. 2008 , 68 , 2842 – 2848 .
• [32] Bian, C. L. ; Zeng, Q. X. ; Yang, L. J. ; Xiong, H. Y. ; Zhang, X. H. ; Wang, S. F. Sensor. Actuat. B-Chem. 2011 , 156 , 615 – 620 .
• [33] Gao L. ; Chen, L. G. Microchim. Acta 2013 , 180 , 423 – 430 .
• [34] Oluwaseun, A. O. ; Vincent, O. N. ; Bice, S. M. ; Sreekantha, B. J. RSC Adv. 2016 , 6 , 2731 – 2745 .
• [35] Laszlo, K. ; Podkoscielny, P. ; Dabrowski, A. Langmuir 2003 , 19 , 5287 – 5294 .
• [36] Fierro, V. ; Torné-Fernández, V. ; Montané, D. ; Celzard, A. Micropor. Mesopor. Mat. 2008 , 111 , 276 – 284 .

Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).