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High Pressure Synthesis versus Calcination – Different Approaches to Crystallization of Zirconium Dioxide

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Calcination and microwave-assisted hydrothermal processing of precipitated zirconium dioxide are compared. Characterization of synthesized products of these two technologies is presented. The infiuence of thermal treatment up to 1200oC on the structural and spectroscopic properties of the so-obtained zirconium dioxide is examined. It was found that initial crystallization of material inhibits the crystal growth up to the 800oC (by means of XRD and TEM techniques), while the material crystallized from amorphous hydroxide precursor at 400oC, exhibits 26 nm sized crystallites already. It was found using the TG technique that the temperature range 100–200oC during the calcination process is equivalent to a microwave hydrothermal process by means of water content. Mass loss is estimated to be about 18%. Based on X-ray investigations it was found that the initial hydroxide precursor is amorphous, however, its luminescence activity suggests the close range ordering in a material.
Rocznik
Strony
99--105
Opis fizyczny
Bibliogr. 36 poz., rys.
Twórcy
autor
  • Institute of Physics of the Polish Academy of Sciences, al. Lotników 32/46, 02-668 Warsaw, Poland
  • Institute of Physics of the Polish Academy of Sciences, al. Lotników 32/46, 02-668 Warsaw, Poland
autor
  • West Pomeranian University of Technology, Szczecin, Institute of Chemical and Environment Engineering, ul. Pułaskiego 10, 70-322 Szczecin, Poland
autor
  • West Pomeranian University of Technology, Szczecin, Institute of Chemical and Environment Engineering, ul. Pułaskiego 10, 70-322 Szczecin, Poland
  • West Pomeranian University of Technology, Szczecin, Institute of Chemical and Environment Engineering, ul. Pułaskiego 10, 70-322 Szczecin, Poland
autor
  • Institute of Physics of the Polish Academy of Sciences, al. Lotników 32/46, 02-668 Warsaw, Poland
Bibliografia
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  • 14. Wysokowski, M., Motylenko, M., Bazhenov, V.V., Stawski, D., Petrenko, I., Ehrlich, A., Behm, T., Kljajic, Z., Stelling, A.L., Jesionowski, T. & Ehrlich, H. (2013). Poriferan chitin as a template for hydrothermal zirconia deposition, Front. Mater. Sci. 7(3), 248–260. DOI:10.1007/s11706-013-0212-x.
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  • 32. Mondal, A. & Ram, S. (2004). Reconstructive phase formation of ZrO2 nanoparticles in a new orthorhombic crystal structure from an energized porous ZrO(OH)2•xH2O precursor, Ceram. Int. 30, 239–249. DOI: 10.1016/S0272-8842(03)00095-6.
  • 33. Smits, K., Grigorjeva, L., Millers, D., Sarakovskis, A., Grabis, J. & Łojkowski, W. (2011). Intrinsic defect related luminescence in ZrO2, J. Lumin. 131, 2058–2062. DOI: 10.1016/j. jlumin.2011.05.018.
  • 34. Guo, G.Y., Chen, Y.L. & Ying, W.J. (2004). Thermal, spectroscopic and X-ray diffractional analyses of zirconium hydroxides precipitated at low pH values, Mater. Chem. Phys. 84, 308–314. DOI: 10.1016/j.matchemphys.2003.10.006.
  • 35. Zhang, Y.L., Jin, X.J., Rong, Y.H., Hsu, T.Y., Jiang, D.Y. & Shi, J.L. (2006). The size dependence of structural stability in nano-sized ZrO2 particles, Mater. Sci. Eng. A 438–440, 399–402. DOI: 10.1016/j.msea.2006.03.109.
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Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-d09a7b29-0cdc-4fe4-b798-16778eba7c09
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