A novel HPLC method for simultaneous quantification of eleven phenolic antioxidants in commercial personal care and food products which contain extracts of green apple, pomegranate and argan oil

• Autorzy: Moussad Ranim I. , Salam Randa A. Abdel , Hadad Ghada M. , EL Gindy Alaa , Foudah Ahmed I. , Hameed Eman A. Abdel

Identyfikatory

DOI

10.1556/1326.2020.00860

• Języki publikacji: EN

Abstrakty

EN

In this study, a simple, fully validated and rapid reversed-phase HPLC with photodiode array detector method was developed for the simultaneous determination of 11 selected phenolic antioxidants over 33 min in personal care and food samples containing extracts of green apple, pomegranate (Ponica granatum) and argan oil (Argania spinosa). The method was performed using NUCLEODUR C18 column 5 µm particle size and 12.5 cm length. The HPLC mobile phase was prepared as follows, solution A: 1% aqueous acetic acid and solution B: Acetonitrile. The method was gradient at flow rate 1.0 mL/min with a simple mobile phase, minimal sample preparation, and diminished organic solvent usage (3% acetonitrile for almost 90% of the run time). The detection was carried out at 278 nm. The method presented good precision and accuracy with RSD% values ranged between 0.33 and 1.94% and wide linear range. The developed method was successfully applied on 67 personal care and food products present in Egyptian market and can be used for routine screening in laboratory for the regular quality control of the antioxidant content for products containing the mentioned extracts.

Słowa kluczowe

EN

antioxidants; argan oil; green apple; HPLC; pomegranate

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2022
• Tom: Vol. 34, no. 1
• Strony: 77--86
• Opis fizyczny: Bibliogr. 41 poz., rys., tab.

Twórcy

autor

Moussad Ranim I.

• Common Laboratories, Ministry of Health, Damietta, Egypt

autor

Salam Randa A. Abdel

• Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Suez Canal University, Ismailia, Egypt
• Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Sinai University, Kantara Branch, Sinai, Egypt

autor

Hadad Ghada M.

• Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Suez Canal University, Ismailia, Egypt

autor

EL Gindy Alaa

• Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Suez Canal University, Ismailia, Egypt

autor

Foudah Ahmed I.

• Department of Pharmacognosy, College of Pharmacy, Prince Sattam Bin Abdulaziz University, AlKharj, Saudi Arabia

• https://orcid.org/0000-0002-6728-8614

autor

Hameed Eman A. Abdel

• Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Port Said University, Port Said, Egypt

Bibliografia

• 1. Ayse, K.; Beraat, O.; Samim, S. Food. Anal. Methods 2009, 241.
• 2. Liu, C.; Wang, J.; Yang;Y. Anal. Methods. 2014, 6, 6038.
• 3. Hirose, M.; Takesada, Y.; Tanaka, H.; Tamano, S.; Kato, T.; Shirai, T. Carcinogenesis 1998, 1, 207.
• 4. Brewer, M. S. Compr. Rev. Food Sci. 2011, 10, 221.
• 5. Yuri, J. A. ; Neira, A. ; Maldonado, F. ; Quilodrán, A. ; Simeone, D. ; Razmilic, I. ; Palomo, I. J. Appl. Bot. Food Qual. 2014, 87 131.
• 6. Francini, A.; Sebastiani, L. Antioxidants 2013, 2181.
• 7. Lutz, M. ; Hernández, J. ; Henríquez, C. J. Food 2015 13 541.
• 8. Can, Z.; Dincer, B.; Sahin, H.; Baltas, N.; Yildiz, O.; Kolayli, S. J. Enzyme Inhib. Med. Chem. 2014, 6, 829.
• 9. Cao, J.; Chen, W.; Zhang, Y.; Zhao, X. Food Sci. Technol. Res. 2010, 5, 395.
• 10. Fischer, U. A.; Carle R., Kammerer, D. R. Food Chem. 2011, 127, 807.
• 11. Mena, P.; Calani, L.; Dall'Asta, C.; Galaverna, G.; Viguera C.; Bruni R.; Crozier A.; Rio, D. Molecules 2012, 17, 14821.
• 12. Zougagh, M.; Salghi, R.; Dhair S.; Rios. A. Anal. Bioanal. Chem. 2011, 399, 2395.
• 13. Khallouki, F.; Haubner, R.; Ricarte, I.; Erben, G.; Klika, K.; Ulrich, M. C.; Owen, R. W. Food Chem. 2015, 179, 191.
• 14. Wojdyło, A.; Oszmiański, J. Antioxidants 2, 9, 567.
• 15. Xuelian Bai, A.; Huawei Zhang, B.; Huang Ren, C. S. J. Sci. Food Agric. 2013, 93, 2502.
• 16. Mindaugas, L.; Pranas, V.; Valdas J., Raimondas, R.; Darius, K.; Arvydas, M.; Valdimaras, J. J. Chem. 2014, 1, 10.
• 17. Bai, X.; Zhang, H.; Ren, S. J. Sci. Food Agric. 2013, 10, 2502.
• 18. Schieber, A.; Keller, P.; Carle, R. J. Chromatogr. A. 2001, 2, 265.
• 19. Riekstina-Dolge, R.; Kruma, Z.; Dimins, F.; Straumite, E.; Karklina, D. Proc. Latv. Univ. Agric. 2014, 31, 326.
• 20. Rabaneda, F.; Jauregui, O.; Raventos, R., Viladomat, F.; Bastida, J.; Codina, C.; Mass Spectrom. 2004, 18, 553.
• 21. Rupasinghe, H.; Kean, C. Can. J. Plant Sci. 2008, 41, 188.
• 22. Rigo, A.; Tonon, D.; Mattivi, F.; Vrhovesk, U. J. Agric. Food Chem. 2004, 21, 6532.
• 23. Montero, L. ; Herrero, M. ; Ibáñez, L. ; Cifuentes, A. J. Chromatogr. A 2013, 1313, 275.
• 24. Wong-paz, J.; Aguilar, C.; Marquez, D.; Guyot S. Food Sci. Technol. 2015, 2, 1091.
• 25. Ma, J.; Yang, H.; Basille, M.; Kennelly, E. J. Agric. Food Chem. 2004, 52, 5873.
• 26. Andrews, P. K.; Reganold, J. P.; Davies, N. M.; Lange, B. M.; Cuthbertson, D. J. Agric. Food Chem. 2012, 35, 8552.
• 27. Mehrizi, R. Z.; Emam-Djomeh, Z.; Shahedi, M; Keramat, J; Rezaei, K; Loni, E. J. Food Qual. Hazards Control 2017, 4, 103.
• 28. Ali, S. I.; El-Baz, F. K; El-Emary, G. A.; Khan, E. A., Mohamed, A. A. Int. J. Pharm. Clin. Res. 2014, 4, 348.
• 29. Zaki, S.A.; Abdelatif, S. H.; Abdelmohsen, N. R.; Ismail, F.A. Int. J. Food Eng. 2015, 1, 1212.
• 30. Mansour, E.; BenKhaled, A.; Lachiheb, B; Abid, M.; Bachar, Kh.; Ferchichi, A. J. Agr. Sci. Tech. 2013, 15, 1393.
• 31. Saxena, R.; Sharma, R; Nandy, B. C. Int. Res. J. Pharm. 2017, 1, 8. 32. Hmid, I.; Elothmani, D.; Hanine, H.; Oukabli, A.; Mehinagi, C. E. Arab. J. Chem. 2013, 2, 2675.
• 32. Hmid, I.; Elothmani, D.; Hanine, H.; Oukabli, A.; Mehinagi, C. E. Arab. J. Chem. 2013, 2, 2675.
• 33. Middha, S. K.; Talambedu, U.; Pande, V. Adv. Pharm. Sci. 2013, 1–6.
• 34. Al-Rawahi, A.;Edwards, G.; Al-Sibani, M. Eur. J. Med. Plants 2014, 3, 315.
• 35. Rojas, L. B.; Quideau, S.; Pardon, P.; Charrouf, Z. J. Agric. Food Chem. 2005, 53, 9122.
• 36. Rabie, K.; Mourad, K.; El Jemli, M. J. Chem. Pharm. Res. 2016, 8, 173.
• 37. Khallouki, F. Eur. J. Cancer Prev. 2003, 12, 67–75.
• 38. El Monfalouti, H; Charrouf, Z; Belvis, S.; Ghirardello, D.; Scursatone, B.; Guillaume, D.; Denhez, C.; Zeppa, G. Eur. J. Lipid Sci. Technol. 2012, 114, 446.
• 39. Bakour, M.; Soulo, N.; Hammas, N. Int. J. Mol Sci. 201819610.
• 40. Hadad, G. M.; AbdelSalam, R. A.; Soliman, R. M.; Mesbah, M. K. Talanta 2012, 10138.
• 41. International Conference on Harmonisation of Technical Requirements for Registration of Pharmaceuticals for Human Use, ICH Harmonised TripartiteGuideline —Validation of Analytical Procedures: Text and Methodology Q2(R1); Current Step 4 version: London, 2005.

Uwagi

Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023).