Preparation of Nickel Nanoparticles Using Nickel Raffinate Separated by Solvent Extraction from The Spent FeCl3 Etching Solution

• Autorzy: Park Il-Jeong , Swain Basudev , Kim Dae-Weon , Kim Geon-Hong , Han Deok-Hyun , Jung Hang-Chul

Identyfikatory

DOI

10.24425/amm.2019.127572

• Języki publikacji: EN

Abstrakty

EN

FeCl₃ bearing etching solution is mainly used for etching of metals used in shadow masks, PCBs and so on. Due course of Invar alloy etching process the FeCl₃ bearing etching solution get contaminated with Ni²⁺ which affect adversely the etching efficiency. Hence, FeCl₃ bearing etching solution discarded after several cycle of operation causes an environmental and economic problem. To address both the issues the etching solution was purified through solvent extraction and remained Ni²⁺ recovered by wet chemical reduction using hydrazine. For optimum Fe³⁺ extraction efficiency, various extraction parameter were optimized and size and morphology of the recovered pure Ni powder was analyzed. The reported process is a simple process to purify and recover Ni from industry etching solution.

Słowa kluczowe

EN

nickel; recycling; solvent extraction; chemical reduction

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2019
• Tom: Vol. 64, iss. 2
• Strony: 531--534
• Opis fizyczny: Bibliogr. 10 poz., fot., rys., tab.

Twórcy

autor

Park Il-Jeong

• Institute for Advanced Engineering (IAE), Yongin, South Korea

autor

Swain Basudev

• Institute for Advanced Engineering (IAE), Yongin, South Korea

autor

Kim Dae-Weon

• Institute for Advanced Engineering (IAE), Yongin, South Korea

autor

Kim Geon-Hong

• Institute for Advanced Engineering (IAE), Yongin, South Korea

autor

Han Deok-Hyun

• Institute for Advanced Engineering (IAE), Yongin, South Korea

autor

Jung Hang-Chul

• Institute for Advanced Engineering (IAE), Yongin, South Korea

Bibliografia

• [1] R. J. Lewis Sr., D. Sax’s Dangerous Properties of Industrial Materials, 8th Ed., Van Norstrand Reinhold, New York (1992).
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• [5] G. L. Pashkov, N. A. Grigorieva, N. I. Pavlenko, I. Y. Fleitlikh, L. K. Nikiforova, M. A. Pleshkov, Solvent Extr. Ion Exch. 26, 749 (2008).
• [6] J. G. Ahn, J. W. Ahn, M. S. Lee, J. Kor. Inst. Met. & Mater. 40, 799 (2002).
• [7] F. Wang, Z. C. Zhang, Z. Q. Chang, J. Mater. Lett. 55, 27 (2002).
• [8] Z. Gui, R. Fan, W. Mo, X. Chen, L. Yang, Y. Hu, J. Mater. Res. Bull. 38, 169 (2003).
• [9] I. J. Park, D. W. Kim, G. H. Kim, H. J. Chae, S. W. Lee, H. C. Jung, Clean Technol. 23, 279 (2017).
• [10] I. J. Park, D. W. Kim, G. H. Kim, H. J. Chae, H. C. Jung, Arch. Metall. Mater. 63, 1441 (2018).

Uwagi

EN

1. This work was supported by the Korea Institute of Energy Technology Evaluation and Planning (KETEP) and the Ministry of Trade, Industry & Energy (MOTIE) of the Republic of Korea (No. 20165020301150, No. 20165020101280).

PL

2. Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).