Structural and thermal properties of Zn-containing magnesium aluminate spinels obtained by wet chemical method

• Autorzy: Kaygili Omer , Bulut Niyazi , Ates Tankut , Ercan Ismail , Koytepe Suleyman , Seckin Turgay , Tatar Cengiz , Gunduz Bayram , Kebiroglu Hanifi

Identyfikatory

DOI

10.2478/msp-2019-0018

• Języki publikacji: EN

Abstrakty

EN

In the present study, the dopant effect of Zn on the crystal structure, thermal properties and morphology of magnesium aluminate (MgAl₂O₄) spinel (MAS) structure was investigated. A pure and two Zn-containing MASs (e.g. MgAl_1.93Zn_0.07O<sub4</sub> and MgAl_1.86Zn_0.14O<sub4</sub>) were synthesized for this purpose via a wet chemical method, and the as-prepared samples were characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, differential thermal analysis (DTA), thermogravimetric analysis (TGA), scanning electron microscopy (SEM) and energy dispersive X-ray (EDX) spectroscopy techniques. It was found that the crystal structure, thermal properties and morphology of the MAS system change with the increase in the amount of Zn. MgO phase formation was observed. The values of the lattice parameter, unit cell volume and crystallite size increased, and the crystallinity percentage decreased. The morphology was also affected by adding of Zn.

Słowa kluczowe

EN

spinel; wet chemical method; crystal structure; thermal properties; morphology

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2019
• Tom: Vol. 37, No. 2
• Strony: 238--243
• Opis fizyczny: Bibliogr. 37 poz., rys., tab.

Twórcy

autor

Kaygili Omer

• Department of Physics, Faculty of Science, Firat University, 23119, Elazig, Turkey

autor

Bulut Niyazi

• Department of Physics, Faculty of Science, Firat University, 23119, Elazig, Turkey

autor

Ates Tankut

• Department of Physics, Faculty of Science, Firat University, 23119, Elazig, Turkey

autor

Ercan Ismail

• Department of Biophysics, Institute for Research and Medical Consultations, Imam Abdulrahman Bin Faisal University, 34441, Dammam, Saudi Arabia

autor

Koytepe Suleyman

• Department of Chemistry, Faculty of Arts & Science, Inonu University, 44280, Malatya, Turkey

autor

Seckin Turgay

• Department of Chemistry, Faculty of Arts & Science, Inonu University, 44280, Malatya, Turkey

autor

Tatar Cengiz

• Department of Physics, Faculty of Science, Firat University, 23119, Elazig, Turkey

autor

Gunduz Bayram

• Department of Science Education, Faculty of Education, Mus Alparslan University, 49250, Mus, Turkey

autor

Kebiroglu Hanifi

• Department of Physics, Faculty of Science, Firat University, 23119, Elazig, Turkey

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).