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Analiza krystalizacji stopów AM60 i AZ91 w formie ceramicznej metodą analizy termiczno-derywacyjnej (ATD)
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Abstrakty
The work presents the test results of the crystallisation and cooling of magnesium alloys: AM60 and AZ91, with the use of the TDA method. The tested alloys were cast into ceramic shells heated up to 180°C, produced according to the technology of the shell production in the investment casting method. The TDA method was applied to record and characterize the thermal effect resulting from the phase transformations occurring during the crystallisation of magnesium alloys. The kinetics and dynamics of the thermal processes of the crystallisation of AM60 and AZ91 in the ceramic shells were determined. Metallographic tests were performed with the use of an optical microscope as well as scanning microscopy, together with the EDS chemical analysis of the phases present in the tested casts. A comparison of these test results with the thermal effect recorded by way of the TDA method was made.
W pracy przedstawiono wyniki badań krystalizacji i stygnięcia stopów magnezu: AM60 i AZ91 przy użyciu metody ATD. Badane stopy zalewano do form ceramicznych podgrzanych do temperatury 180°C, wykonanych zgodnie z technologią wytwarzania form w metodzie traconych modeli. Przy pomocy metody ATD zarejestrowano i wyznaczono charakterystyczne efekty cieplne wynikające z przemian fazowych zachodzących podczas krystalizacji badanych stopów magnezu. Określono kinetykę i dynamikę procesów cieplnych krystalizacji stopów AM60 i AZ91 w formach ceramicznych. Przeprowadzono badania metalograficzne przy pomocy mikroskopu optycznego oraz mikroskopii skaningowej wraz z analizą chemiczną EDS występujących faz w badanych odlewach. Porównano wyniki tych badań z efektami cieplnymi zarejestrowanymi metodą ATD.
Wydawca
Czasopismo
Rocznik
Tom
Strony
1449--1455
Opis fizyczny
Bibliogr. 14 poz., rys., tab.
Twórcy
autor
- Lodz University of Technology, Department of Materials Engineering and Production Systems, 1 Stefanowskiego Str., 90-924 Łódź, Poland
autor
- Lodz University of Technology, Department of Materials Engineering and Production Systems, 1 Stefanowskiego Str., 90-924 Łódź, Poland
autor
- Foundry Research Institute, 73 Zakopianska Str., 30-418 Kraków, Poland
autor
- Lodz University of Technology, Department of Materials Engineering and Production Systems, 1 Stefanowskiego Str., 90-924 Łódź, Poland
Bibliografia
- [1] G. Gumienny, Carbidie Bainitic and Ausferritic Ductile Cast Iron. Archives of Metallurgy and Materials 58(4), 1053-1058 (2013).
- [2] G. Gumienny, Bainitic-martensitic nodular cast iron with carbides, Archives of Foundry Engineering 10, 2, 63-68 (2010).
- [3] S. Pietrowski, B. Pisarek, Computer-aided technology of melting high-quality metal alloys, Archives of Metallurgy and Materials 52, 3, 481-486 (2007).
- [4] B. Pisarek, Influence of the technology of melting and inoculation preliminary alloy AlBe5 on change of concentration of Al and micro-structure of the bronze CuAl10Ni5Fe4. Archives of Foundry Engineering 10, 2, 127-134 (2010).
- [5] S. Jura, Z. Jura, Theory of ATD method in tests of Al alloys, Solidification of Metals and Alloys 28, PAN Katowice, 57-88 (1996) (in Polish).
- [6] R. Wladysiak, Effect of water mist on cooling process of casting die and microstructure of AlSi11 alloy, Archives of Metallurgy and Materials 55(3), 939-946 (2010).
- [7] S. Pietrowski, T. Szymczak, Crystallisation, microstructure and mechanical properties of silumins with micro-additions of Cr, Mo, W and V, Archives of Foundry Engineering 10, 1, 123-136 (2010).
- [8] L. A. Dobrzański, T. Tański, A.D. Dobrzańska-Danikiewicz, M. Król, S. Malara , J. Domagała-Dubiel, The microstructure and properties of alloys of Mg-Al-Zn, Chapter 3 The derivative thermal analysisof Mg-Al-Zn Open Access Library 5 (11), 44-77 (2012) (in Polish).
- [9] B. Nami, S. G. Shabestaria, S. M . Miresmaeili, H. Razavi, Sh. Mirdamadi, The effect of rare earth elements on the kinetics of the isothermal coarsening of the globular solid phase in semisolid AZ91 alloy produced via SIMA process, Journal of Alloys and Compounds 489, 570-575 (2010).
- [10] S. Lun Sin, D. Dube, R. Tremblay, An investigation on microstructural and mechanical properties of solid mould investment casting of AZ91D magnesium alloy, Materials Characterization 59, 178-187 (2008).
- [11] H. Jafari, M. H. Idris, A. Ourdjini, M. R. Abdul Kadir, Effect of Flux on In-Situ Melting Shell Investment Casting of AZ91D Magnesium Alloy, International Conference on Thermal, Material and Mechanical Engineering (ICTMME’ 2012) July 15-16, Singapore, 143-148 (2012).
- [12] Y . Zhiyong, Z. Yuhua, Ch. Weili, Z. Jinshan, W. Yinghui, Effect of Cu addition on microstructure and properties of Mg-10Zn-5Al-0.1Sb high zinc magnesium alloy, China Foundry, Research & Development, February, 43-47 (2012).
- [13] S. Pietrowski, C.Rapiejko, Temperature and microstructure characteristics of silumin casting AlSi9 made with investment casting method, Archives of Foundry Engineering 11, 3, 177-186 (2011).
- [14] A. Maltais, D. Dube, M. Fiset, G. Laroche, S. Turgeon, Improvements in the metallography of as-cast AZ91 alloy, Material Characterization 52, 103-119 (2004).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-c22b3f80-a8cc-4a07-b56e-d3b8231b9ef9