Determination of acrylamide in foods by automatic accelerated solvent extraction and gas chromatography-mass spectrometry

• Autorzy: Kang Cuicui , Ma Haijian , Li Yuan , Zhang Chizhong , Hong Yueqin , Shao Minghua

Identyfikatory

DOI

10.1556/1326.2020.00755

• Języki publikacji: EN

Abstrakty

EN

The aim of the experiment is to establish a method for the determination of acrylamide in food by automatic accelerated solvent extraction-gas chromatography-mass spectrometry. D3-acrylamide was used as isotope internal standard, crushed samples were extracted and purified by automatic accelerated solvent, acrylamide was derivatized into 2,3-dibromopropanamide by potassium bromide and potassium bromate under acidic conditions, and then the derivative was extracted by ethyl acetate and detected by gas chromatography-mass spectrometry. The method had a good linear relationship in the concentration range of 10–2000 ng/mL, and the coefficient of determination (R2) was 0.9997. The detection limit of the method was 3 mg/kg. The quantification limit of the method was 10 mg/kg. The standard addition recovery of acrylamide was between 105 and 120%, and the relative standard deviation of the recovery of acrylamide was less than 3.0%. The experimental result showed that the method was simple, sensitive, efficient and accurate, and could be used for the determination of acrylamide in food.

Słowa kluczowe

EN

acrylamide; automatic accelerated solvent extraction; gas chromatography-mass spectrometry; baked and fried foods

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2021
• Tom: Vol. 33, no. 1
• Strony: 64--72
• Opis fizyczny: Bibliogr. 40 poz., rys., tab.

Twórcy

autor

Kang Cuicui

• ANPEL Laboratory Technologies (Shanghai) Inc., Yezhang Road 59, Shanghai, 2016600, China

autor

Ma Haijian

• ANPEL Laboratory Technologies (Shanghai) Inc., Yezhang Road 59, Shanghai, 2016600, China

• https://orcid.org/0000-0002-4415-4541

autor

Li Yuan

• ANPEL Laboratory Technologies (Shanghai) Inc., Yezhang Road 59, Shanghai, 2016600, China

autor

Zhang Chizhong

• ANPEL Laboratory Technologies (Shanghai) Inc., Yezhang Road 59, Shanghai, 2016600, China

autor

Hong Yueqin

• ANPEL Laboratory Technologies (Shanghai) Inc., Yezhang Road 59, Shanghai, 2016600, China

autor

Shao Minghua

• ANPEL Laboratory Technologies (Shanghai) Inc., Yezhang Road 59, Shanghai, 2016600, China

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Uwagi

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).