Silver nanoparticles deposited on calcium hydrogenphosphate – silver phosphate matrix; biological activity of the composite

• Autorzy: Szmuc K. , Kus-Liskiewicz M. , Szyller Ł. , Szmuc D. , Stompor M. , Zawlik I. , Ruman T. , Wołowiec S. , Cebulski J.

Identyfikatory

DOI

10.2478/pjct-2019-0013

• Języki publikacji: EN

Abstrakty

EN

The composite containing nanosilver uniformly deposited on matrix composed of CaHPO₄  x 2H₂ O (brushite, ca 89 mass %), CaHPO₄  (monteonite, ca 9.5 mass%), and Ag₃ PO₄  (0.5 mas%) was obtained by addition of calcium nitrate and silver nitrate aqueous solution at 30:1 Ca:Ag molar ratio into excess of (NH₄ )₂ PO₄  solution at pH 5.0 – 5.5. The isolated solid was characterized by STEM, XRD, and LDI mass spectrometry. It has been found that nanosilver was uniformly distributed within composite as <10 nm diameter sized nanoparticles. Determination of silver by AAS showed that 60% of silver is present as Ag(0) nanoparticles, the present as matrix Ag₃ PO₄  as identified by XRD method. The composite showed strong growth inhibition in E. coli and P. aeruginosa strains, and moderate towards S. aureus. The C. albicans cells were the most resistant to the tested material, although still composite was moderately cytostatic for the yeast.

Słowa kluczowe

EN

silver nanoparticles; composite; calcium hydrogenphosphate matrix; electron microscopy; mass spectrometry

• Wydawca: West Pomeranian University of Technology. Publishing House
• Czasopismo: Polish Journal of Chemical Technology
• Rocznik: 2019
• Tom: Vol. 21, nr 2
• Strony: 6--13
• Opis fizyczny: Bibliogr. 34 poz., rys., tab.

Twórcy

autor

Szmuc K.

• University of Rzeszów, Faculty of Mathematics and Natural Sciences, 16c Rejtana Ave., 35-959 Rzeszów, Poland
• Rzeszów University of Technology, Faculty of Chemistry, 6 Powstańców Warszawy Ave. 35-959 Rzeszów, Poland

autor

Kus-Liskiewicz M.

• University of Rzeszów, Faculty of Biotechnology, 16c Rejtana Ave., 35-959 Rzeszów, Poland

autor

Szyller Ł.

• University of Rzeszów, Faculty of Mathematics and Natural Sciences, 16c Rejtana Ave., 35-959 Rzeszów, Poland

autor

Szmuc D.

• Rzeszów University of Technology, Faculty of Chemistry, 6 Powstańców Warszawy Ave. 35-959 Rzeszów, Poland

autor

Stompor M.

• University of Rzeszów, Faculty of Medicine, 16c Rejtana Ave., 35-959 Rzeszów, Poland
• Rzeszów University of Technology, Faculty of Chemistry, 6 Powstańców Warszawy Ave. 35-959 Rzeszów, Poland

autor

Zawlik I.

• University of Rzeszów, Faculty of Medicine, 16c Rejtana Ave., 35-959 Rzeszów, Poland
• Rzeszów University of Technology, Faculty of Chemistry, 6 Powstańców Warszawy Ave. 35-959 Rzeszów, Poland

autor

Ruman T.

• Rzeszów University of Technology, Faculty of Chemistry, 6 Powstańców Warszawy Ave. 35-959 Rzeszów, Poland

autor

Wołowiec S.

• University of Rzeszów, Faculty of Medicine, 16c Rejtana Ave., 35-959 Rzeszów, Poland
• Rzeszów University of Technology, Faculty of Chemistry, 6 Powstańców Warszawy Ave. 35-959 Rzeszów, Poland

autor

Cebulski J.

• University of Rzeszów, Faculty of Mathematics and Natural Sciences, 16c Rejtana Ave., 35-959 Rzeszów, Poland
• Rzeszów University of Technology, Faculty of Chemistry, 6 Powstańców Warszawy Ave. 35-959 Rzeszów, Poland

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Uwagi

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).

Poz. 26 w bibliografii zawiera dodatkowo poz., 26 a i 26 b.