Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction

• Autorzy: Mohamad Mardawani , Ibrahim H. A. , Nasir M. F. M. , Mohidem Nur Atikah , Shoparwe N. F. , Teo Pao Ter , Masri Mohamad Najmi , Irfan Abd Rahim

Identyfikatory

DOI

10.24425/amm.2022.139703

• Języki publikacji: EN

Abstrakty

EN

Tannic acid or tannin, type of phenolic compound contains in kenaf bast fibre. Conventional extraction has certain limitations in terms of time, energy, and solvent consumption. Ultrasound assisted extraction (UAE) can extract bioactive components in shorter time, low temperature, with lesser energy and solvent requirement. UAE as alternative extraction technique is better equipped to retain the functionality of the bioactive compounds. In this study, the conditions for ultrasound assisted extraction (UAE) of tannic acid from kenaf bast fibre by assessing the effect of sonication time and different duty cycles were optimized. The use of ultrasound to extract tannic acid from kenaf bast fiber was evaluated. Ultrasound-assisted extraction (UAE) was carried out using ethanol as solvent to intensify the extraction efficacy. Phytochemical screening was conducted to identify the presence of tannic acid in extracts. The extracts then were analyzed using High-Performance Liquid Chromatography (HPLC) and Scanning Electron Microscopy (SEM). It was found that 0.2429 mg/mL of tannic acid was obtained under the extraction conditions of extraction temperature of 40℃, sonication time of 20 minutes and duty cycle of 50%. From SEM analysis, it was found that the raw sample demonstrated rough surface and no porous but kenaf bast fibre display smoother surface with less impurities and few pores appeared after the extraction process using UAE. These results indicate that ultrasound-assisted extraction is an efficient method for extracting tannic acid from kenaf bast fibre with the advantages of lower extraction time and higher extraction yield.

Słowa kluczowe

EN

ultrasonic assisted extraction; UAE; sonication time; duty cycle; extraction process; kenaf bast fibre

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2022
• Tom: Vol. 67, iss. 3
• Strony: 1061--1066
• Opis fizyczny: Bibliogr. 26 poz., fot., rys., tab.

Twórcy

autor

Mohamad Mardawani

• Universiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, Malaysia

• https://orcid.org/0000-0003-1376-5232

autor

Ibrahim H. A.

• Universiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, Malaysia

autor

Nasir M. F. M.

• National Kenaf and Tobacco Board, Kubang Kerian, Kelantan, Malaysia

autor

Mohidem Nur Atikah

• Universiti Putra Malaysia, Faculty of Engineering Selangor, Department of Biological and Agricultural Engineering, Malaysia

• https://orcid.org/0000-0001-9892-4823

autor

Shoparwe N. F.

• Universiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, Malaysia

autor

Teo Pao Ter

• Universiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, Malaysia

• https://orcid.org/0000-0002-2012-5981

autor

Masri Mohamad Najmi

• Universiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, Malaysia

• https://orcid.org/0000-0003-2577-6756

autor

Irfan Abd Rahim

• Universiti Malaysia Perlis, Faculty of Mechanical Engineering Technology, Perlis, Malaysia
• Universiti Malaysia Perlis, Center of Excellence Geopolymer and Green Technology (CEGeoGTech), Perlis, Malaysia

• https://orcid.org/0000-0002-6606-9874

Bibliografia

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Uwagi

1. The authors acknowledge the financial support received in the form of grants from the Ministry of 1. Higher Education Malaysia via Prototype Development Research Grant (PRGS), R/PRGS/A1300/01155a/004/2020/00801 and Universiti Malaysia Kelantan through UMK Rising Star 2021 (R/STA/A1300/01155a/006/2021/00927).

2. Opracowanie rekordu ze środków MNiSW, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2024).