Determination of eight kinds of glucocorticoids residues in chicken muscle with on-line clean up combined HPLC-MS/MS

• Autorzy: Yang Yahua , Xue Zhizhong , Meng Ran , Wu Zhe , Li Zhaojia , Zhang Wei , Ge Shihui

Identyfikatory

DOI

10.1556/1326.2021.00933

• Języki publikacji: EN

Abstrakty

EN

A sensitive and rapid method using HPLC-MS/MS was developed for the determination of Wight glucocorticoids residues in chicken muscle simultaneously by Turbo Flow. The eight glucocorticoids were prednisone, prednisolone, hydrocortisone, methylprednisolone, dexamethasone, betamethasone, beclomethasone and fludrocortisones. Samples were extracted with ethyl acetate and on-line cleaned up through a Turbo Flow solid-phase extraction column without time-consuming pretreatment before HPLC-MS/MS analysis. Sample pretreatment conditions, Turbo Flow conditions and mass spectra parameters were optimized and obtained eight glucocorticoids calibration curves. These curves showed good linearity over the concentration from 0.2 mg/kg to 50 mg/kg with an average recovery from 71.63% to 117.36%. This method could be applied on real samples and provided simple, rapid, sensitive and highly selective analysis, which made it feasible to be adopted in food inspection organizations or carry out quantitative analysis for other banned substance.

Słowa kluczowe

EN

glucocorticoid; chicken muscle; Turbo Flow; HPLC-MS/MS; on-line cleanup

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2022
• Tom: Vol. 34, no. 3
• Strony: 267--275
• Opis fizyczny: Bibliogr. 20 poz., rys., wykr.

Twórcy

autor

Yang Yahua

• Institute of Coastal Agriculture, Hebei Academy of Agriculture and Forestry Sciences, Tangshan, 063299, China

autor

Xue Zhizhong

• Hebei Saline Alkali Land Greening Technology Innovation Center, Tangshan, 063299, China

autor

Meng Ran

• Institute of Coastal Agriculture, Hebei Academy of Agriculture and Forestry Sciences, Tangshan, 063299, China

autor

Wu Zhe

• Hebei Saline Alkali Land Greening Technology Innovation Center, Tangshan, 063299, China

autor

Li Zhaojia

• Hebei Saline Alkali Land Greening Technology Innovation Center, Tangshan, 063299, China

autor

Zhang Wei

• Institute of Coastal Agriculture, Hebei Academy of Agriculture and Forestry Sciences, Tangshan, 063299, China

autor

Ge Shihui

• Shijiazhuang Jinbiao Inspection Service Co., Ltd, Shijiazhuang, 050051, China

• https://orcid.org/0000-0001-9373-5652

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