Synthesis of SrTiO3 by the Calcination of SrCO3 and TiO2 Mixtures Intensively Ground by Means of High Energy Milling

• Autorzy: Rocha-Rangel Enrique , Pech-Rodríguez Wilian J. , López-Hernández Juan , Calles-Arriaga Carlos A. , Armendáriz-Mireles Eddie N. , Castillo-Robles José A. , Rodríguez-García José A.

Identyfikatory

DOI

10.24425/amm.2020.132801

• Języki publikacji: EN

Abstrakty

EN

A SrTiO₃ electroceramic with perovskite structure was produced by the calcination of a mixture of SrCO₃ and TiO₂ intensively grounded by high energy milling. For this purpose, raw materials were mixed in stoichiometric amounts in a planetary type mill; the obtained powder mixture was calcined for 2 h at temperatures between 800 and 1300°C. Samples resulting from the calcination were characterized by XRD, FTIR, SEM analysis and electrical measurements. From XRD, it was determined that the SrTiO₃ formed presents the cubic structure of perovskite. The complete reaction for SrTiO₃ compound formation occurs at 1200°C. Micrograph observations indicate the presence of a homogeneous microstructure with tiny grain size. The measured values of electrical resistivity were within the typical range of insulating materials.

Słowa kluczowe

EN

SrTiO3; mechanochemistry; insulating ceramics; perovskite

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2020
• Tom: Vol. 65, iss. 2
• Strony: 621--626
• Opis fizyczny: Bibliogr. 32 poz., fot., rys., tab., wzory

Twórcy

autor

Rocha-Rangel Enrique

• Universidad Politécnica de Victoria, Av. Nuevas Tecnologías 5902, Parque Científico y Tecnológico de Tamaulipas, Ciudad Victoria, Tamaulipas, México

autor

Pech-Rodríguez Wilian J.

• Universidad Politécnica de Victoria, Av. Nuevas Tecnologías 5902, Parque Científico y Tecnológico de Tamaulipas, Ciudad Victoria, Tamaulipas, México

autor

López-Hernández Juan

• Universidad Politécnica de Victoria, Av. Nuevas Tecnologías 5902, Parque Científico y Tecnológico de Tamaulipas, Ciudad Victoria, Tamaulipas, México

autor

Calles-Arriaga Carlos A.

• Universidad Politécnica de Victoria, Av. Nuevas Tecnologías 5902, Parque Científico y Tecnológico de Tamaulipas, Ciudad Victoria, Tamaulipas, México

autor

Armendáriz-Mireles Eddie N.

• Universidad Politécnica de Victoria, Av. Nuevas Tecnologías 5902, Parque Científico y Tecnológico de Tamaulipas, Ciudad Victoria, Tamaulipas, México

autor

Castillo-Robles José A.

• Universidad Politécnica de Victoria, Av. Nuevas Tecnologías 5902, Parque Científico y Tecnológico de Tamaulipas, Ciudad Victoria, Tamaulipas, México

autor

Rodríguez-García José A.

• Universidad Politécnica de Victoria, Av. Nuevas Tecnologías 5902, Parque Científico y Tecnológico de Tamaulipas, Ciudad Victoria, Tamaulipas, México

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Uwagi

PL

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).