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Nanoemulsje na bazie wybranych olejów z nasion owoców jagodowych
Języki publikacji
Abstrakty
The aim of this work was the preparation of O/W nanoemulsions based on supercritical CO2 extracted (SC-CO2) oils from seeds of strawberry and blackcurrant. The emulsion systems were obtained by the phase inversion composition method, at T = 25°C. Polysorbate 80 and Natragem S150 were used as the surfactant and co-surfactant, respectively. Kinetic stability of the prepared formulations with varying surfactant: oil (S:O) and surfactant/co-surfactant (S/CoS) weight ratio, was analysed by measuring the droplet size (DLS method) in time. The obtained results show that a nanoemulsion based on blackcurrant seed oil was characterised by the smallest droplet size (r = 15 nm), a low polydispersity index (PDI = 0.246) and the longest kinetic stability (S:CoS = 8:2, S/CoS:O = 9:1).
Celem pracy było otrzymanie nanoemulsji O/W, w których rolę fazy olejowej pełnił ekstrakt z nasion truskawki lub czarnej porzeczki otrzymany w warunkach nadkrytycznego CO2 (SC-CO2). Układy emulsyjne otrzymano metodą składnikowej inwersji faz, w T = 25°C. Jako surfaktant zastosowano Polisorbat 80, rolę kosurfaktantu pełnił Natragem S150. Kinetyczną stabilność otrzymanych formulacji badano poprzez pomiar wielkości cząstek nanoemulsji (technika DLS) w czasie, dla układów o różnym stosunku wagowym surfaktant: olej (S:O) oraz surfactant/kosurfaktant (S/CoS). Otrzymane rezultaty wykazały, że najmniejszym rozmiarem cząstek fazy wewnętrznej (r = 15 nm), niskim indeksem polidyspersyjności (PDI = 0.246) oraz najdłuższą kinetyczną stabilnością charakteryzowała się nanoemulsja na bazie oleju z nasion czarnej porzeczki (S:CoS = 8:2, S/CoS:O = 9:1).
Czasopismo
Rocznik
Strony
91--100
Opis fizyczny
Bibliogr. 28 poz., tab., wykr.
Twórcy
autor
- Institute of Inorganic Chemistry and Technology, Faculty of Chemical Engineering and Technology, Cracow University of Technology
autor
- Institute of Inorganic Chemistry and Technology, Faculty of Chemical Engineering and Technology, Cracow University of Technology
autor
- Institute of Inorganic Chemistry and Technology, Faculty of Chemical Engineering and Technology, Cracow University of Technology
Bibliografia
- [1] Malinowska O., Szeląg H., The investigation of application possibilities and rheological behavior of crude fruit seed oil in emulsion system, International Journal of Research in Cosmetic Science, Vol. 3(1), 2013, 7–13.
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- [5] Porras M., Solans C., Gonzalez C., Gutierrez J.M., Properties of water–in–oil (W/O) nano–emulsions prepared by a low–energy emulsification method, Colloids and Surfaces A:Physicochem.Eng.Aspects, Vol. 324, 2008, 181–188.
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- [7] Yang H., Cho W., Park S., Stability of oil–in–water nano–emulsions prepared using the phase inversion composition method, Journal of Industrial and Engineering Chemistry, Vol. 15, 2009, 331–335.
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- [21] Hoed V., De Clercq N., Echim C., Andjelkovic M., Leber E., Dewettinck K., Verhé R., Berry seeds: a source of specialty oils with high content of bioactives and nutritionalvalue, Journal of Food Lipids, Vol. 16, 2009, 33–49.
- [22] Sikora E., Michorczyk P., Olszańska M., Ogonowski J., Supercritical CO2 extract from strawberry seeds as a valuable, component of mild cleansing compositions, International Journal of Cosmetic Science, Vol. 37, 2015, 574–578.
- [23] Rój E., Dobrzyńska-Inger A., Kostrzewa D., Kołodziejczyk K., Sój M., Król B., Miszcza A., Markowski J., Extraction of berry seed oils with supercritical CO2, Przemysł Chemiczny, Vol. 88 (12), 2009, 1325–1330.
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- [25] Ostertag F., Weiss J., McClements D.J., Low–energy formation of edible nanoemulsions: Factors influencing droplet size produced by emulsion phase inversion, Journal of Colloid and Interface Science, Vol. 388, 2012, 95–102.
- [26] Li Y., Zhang Z., Yuan Q., Liang H., Vriesekoop F., Process optimization and stability of D–limonene nanoemulsions preapred by catastrophic phase inversion method, Journal of Food Engineering, Vol. 119, 2013, 419–424.
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Typ dokumentu
Bibliografia
Identyfikator YADDA
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