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The results of a microstructure examination and mechanical properties of 15HM (13CrMo4-5) steel are presented in the article. The examined elements are the samples taken from the live steam pipeline serviced for about 420 000 hours at the temperature of about 510°C, and pressure of 11 MPa. It has been shown that after long-term operation the examined steel has a ferritic-pearlitic microstructure with a dominant content of quasipolygonal ferrite. The processes of fragmentation of lamellar precipitates and their spheroidization were observed in pearlite. On the grain boundaries, single lamellar precipitations were observed. Moreover, numerous precipitations at the interface of three grain boundaries were revealed. The examined steel, despite its long-term service time, was characterized by the strength properties (YS, TS) slightly lower than the required minimum, the impact energy value KV equal to 20 J, and the transition temperature shifted to a temperature above zero. Relatively low level of degradation of the microstructure and mechanical properties of the investigated steel can result from high stability of the ferritic-pearlitic microstructure.
Wydawca
Czasopismo
Rocznik
Strony
5--11
Opis fizyczny
Bibliogr. 19 poz., tab., rys.
Twórcy
autor
- Institue of Materials Engineering, Cracow University of Technology, Jana Pawła II 37, 31-864 Cracow, Poland
autor
- Institue of Materials Engineering, Czestochowa University of Technology, Armii Krajowej 19, 42-200 Częstochowa, Poland
autor
- Institue of Materials Engineering, Czestochowa University of Technology, Armii Krajowej 19, 42-200 Częstochowa, Poland
autor
- Welding Departament, Czestochowa University of Technology, Armii Krajowej 19c, 42-200 Częstochowa, Poland
autor
- UDT, W. Przybylaka 8, 41-300 Dąbrowa Górnicza, Poland
autor
- Institue of Materials Engineering, Czestochowa University of Technology, Armii Krajowej 19, 42-200 Częstochowa, Poland
Bibliografia
- 1. Jasiński A.: Extented operational time of domestic power units - chances and threats [in Polish], Energetyka, 3 (2013), 551-556.
- 2. Dobrzański J.: Materials science interpretation of the life of steels for power plants [in Polish], Open Access Library, 3, 2011.
- 3. Dziuba - Kałuża M., Dobrzański J., Zieliński A.: Mechanical properties of Cr-Mo and Cr-Mo-V low-alloy steel welded joints after long-term service under creep conditions, Arch. Mater. Sc. Eng., 63 (2013), 5-12.
- 4. Dobrzański J., Krztoń H., Zieliński A.: Development of the precipitation processes in low-alloy Cr-Mo type steel for evolution of the material state after exceeding the assessed lifetime, J. Achiev. Mater. Manufac. Eng., 2, 23, (2007), 19-22.
- 5. PN-75/H-84024 Steels for elevated temperatures service. Grades.
- 6. PN-EN ISO 643:2012 Steels - Micrographic determination of the apparent grain size.
- 7. Khan S. A., Islam M. A.: Influence of prior austenite grain size on the degree of temper embrittlement in Cr-Mo steel, J. Mater. Eng. Perform., 16, (2007), 80-85.
- 8. Nguyen T. D., Sawada K., Kushima H., Tabuchi M., Kimura K.: Change of precipitation free zone during long - term creep in 2.25Cr-1Mo steel, Mater. Sc. Eng. A, 591A (2014), 130-135.
- 9. Golański G., Pietryka I., Słania J., Jasak J., Urbańczyk P., Microstructure and mechanical properties of welded joint of 12HMF steel after long - term service [in Polish], Welding Technology Review [Przegląd Spawalnictwa], 5, 2014, 49-53.
- 10. Joarder A., Sarma D. S., Cheruvu N. S.: Effect of long - term service exposure on microstructure and mechanical properties of a CrMoV steam turbine rotor steel, Metall. Trans., 22A (1991), 1811-1820.
- 11. Pigrova P. G.: Carbide diagrams and precipitation of alloying elements during aging of low-alloy steels, Metall. Mater. Trans. A, 27 (1996), 498-502.
- 12. Janovec J., Svoboda M., Vyrostkova A., Kroupa A.: Time-temperature-precipitation diagrams of carbide evolution in low alloy steels, Mater. Sc. Eng., 402A (2005), 288-293.
- 13. Stevens R. A., Flewitt P. E. J.: The effect of phosphorus on the microstructure and creep properties of 2¼%Cr1%Mo steel, Acta Metall., 5 (1986), 849-866.
- 14. Dobrzański J., Hernas A.: Correlation between phase composition and life-time of 1Cr-0.5Mo steels during long-term service at elevated temperatures, J. Mater. Proces. Technol., 53 (1995), 101-108.
- 15. Afrouz A., Collins M. J., Pilikngton R.: Microstructural examination of 1Cr-0.5Mo steel during creep Met. Technol., 12 (1983), 461-463.
- 16. Stachura S., Stradomski Z., Golański G.: Phosphorus in ferroalloys [in Polish], Hutnik - Wiadomości Hutnicze, 5 (2001), 184-193.
- 17. Janovec J.: Nature of alloy steel intergranular embrittlement, Veda Publ., Bratislava, 1999.
- 18. Islam M. A., Novovic M., Bowen P., Knott J.F.: Effect of phosphorus segregation on fracture properties of 2.25Cr-1Mo pressure vessel steel, J. Mater. Eng. Perform., 12, 3 (2003), 244-248.
- 19. Suzuki S., Obata M., Abiko K., Kimura H.: Effect of carbon on the grain boundary segregation of phosphorus in α - iron, Sc. Metall. 17 (1983), 1325-1328.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-b63a720d-5262-4bb1-adf5-12e335895908